Determination of Trace Impurity Elements in the Li-Pb Alloy
Rare Metals and Cemented Carbides | Vol., Issue 3, 2009 |
pp. 29-32
The content of trace impurity elements-Fe,Na,Al, Mg-in the alloy Li17 Pb83 was measured by inductively coupled plasma emission spectroscopy (ICP-AES). The optimization of measuring parameters was explored as well as the type and dosage of acid. And the interference effect of coexistent elements on the analysis result was also studied. The results show that the mass fractions of Fe,Na,AI,Mg in Li17Pb83 are respectively 0. 003%,0. 005 8%,0. 002 6% and 0. 002% ,when carrier gas pressure is 0.25 MPa,generator power 1.3 k W,observation height 10 mm above the coil, the volume ratio of hydrochloric acid to nitric acid 4 : 1 and the total acid concentration 10%.
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