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Hydroxide Co-precipitation-Spectrophotometry of Total RE in Ion-sorption Type Ores

Rare Metals and Cemented Carbides | Vol., Issue 1, 1997 | pp. 44-48
The determination method has the following steps: RE hydroxides co-precipitation,while Fe, Al, Ca,etc,are masked; masking the small amount of the co-precipitatedimpurities; developing with arsenazo N at PH 2. 2~3. 01 direct determination with spectrophotometry. The determination range is 0-50μg/mL X 25' Coefficent of variance 2. 2%.Recovery (100±3. 2) %.
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Thermodynamic Behavior of Materials during Crushing and their Influence on Oxygen Content of the Na-reduced Ta Powder

Rare Metals and Cemented Carbides | Vol., Issue 4, 1996 | pp. 1-6
As a matter of record, using the thermodynamic theory ofmaterial crushing, the process of crushing of Ta lump is analysed. Itshoals the etistenc3 a-catty tiings of lit3tantaneous high temperature i'crushing process in open--type e4uipment, which resu its in format ionof Ta oxide and oxynitride .Oxygen enrichment of Ta powder from thisoperation is estimated and discussed. The conclusion is that crushingprocess of the Na--reduced Ta lump is a oxygen enriched one. so w.must give the matter thought.
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Coprecipitation Preparation and Characterization of Mixed Rare Earth Oxide Fine Powders

Rare Metals and Cemented Carbides | Vol., Issue 4, 1996 | pp. 8-12
Using rare earth oxide(RE 95%)as raw material. mixed rareearth oxide fine powders were prepared by coprecipitation method inwhich urea--aqua ammonia adhere tised to adjtlst the system PH in heatedsolution. The in f luences of preparation condition for products werediscussed init laily. The f me poal-ders were character lied by thermogravimetric, differential thermal analysis, sweep electron microscope,infrared spectrum. The result sho-tvs that mixed rare earth oxide finepowders can be obtained. and under the selected conditions its gra in sizeis about 1  ̄1. 5μm.
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