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Study on Thermal Stability of γ-Al2O3 Powders Modified by Samarium Doping AITranslate

School of Petrochemical Engineering,Liaoning Petrochemical University;School of Petrochemical Engineering,Liaoning Petrochemical University;School of Petrochemical Engineering,Liaoning Petrochemical University;School of Petrochemical Engineering,Liaoning Petrochemical University;School of Petrochemical Engineering,Liaoning Petrochemical University;School of Petrochemical Engineering,Liaoning Petrochemical University;School of Petrochemical Engineering,Liaoning Petrochemical University
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Publisher: Editorial Office of Rare Metals and Cemented Carbides
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Abstract AITranslate

Using aluminum nitrate(Al(NO3)3·9H2O)as the oxidizing agent,glycine(C2H5NO2)as the reducing agent,and samarium nitrate(Sm(NO3)3·6H2O)as the modifier,γ-Al2O3 powders were synthesized by solution combustion method.The products were characterized by XRD,SEM,BET and TG-DTG.The effects of roasting temperature and modifier addition on the phase of the products were analyzed and discussed.The experimental results show that theγ-Al2O3 powders with high thermal stability could be prepared under the molar ratio of aluminum nitrate(Al(NO3)3·9H2O)to glycine(C2H5NO2)of 3∶5,addition of modifier Sm(NO3)3·6H2O of 1%,roasting temperature of 1025℃,and roasting time of 4 h.And theγ-Al2O(3)powders have the characteristics of large specific surface area and stable structure,which can be used as the carrier of catalyst.

KeyWords AITranslate

solution combustion method samarium doping samarium nitrate γ-Al2O3 modification thermal stability

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DOI:

Chinese Library Classification Number:TQ132.2[化学工程—无机化工]

Citation Information:

Using aluminum nitrate(Al(NO3)3·9H2O)as the oxidizing agent,glycine(C2H5NO2)as the reducing agent,and samarium nitrate(Sm(NO3)3·6H2O)as the modifier,γ-Al2O3 powders were synthesized by solution combustion method.The products were characterized by XRD,SEM,BET and TG-DTG.The effects of roasting temperature and modifier addition on the phase of the products were analyzed and discussed.The experimental results show that theγ-Al2O3 powders with high thermal stability could be prepared under the molar ratio of aluminum nitrate(Al(NO3)3·9H2O)to glycine(C2H5NO2)of 3∶5,addition of modifier Sm(NO3)3·6H2O of 1%,roasting temperature of 1025℃,and roasting time of 4 h.And theγ-Al2O(3)powders have the characteristics of large specific surface area and stable structure,which can be used as the carrier of catalyst.

quote

GB/T 7714-2015 [1] WANG Li-ming, JIA Ya-wei, MENG Zhu, et al. Study on Thermal Stability of γ-Al2O3 Powders Modified by Samarium Doping[J]. Rare Metals and Cemented Carbides, 2023(3): 47-51.
MLA [1] WANG Li-ming, et al., "Study on Thermal Stability of γ-Al2O3 Powders Modified by Samarium Doping." Rare Metals and Cemented Carbides, no. 3, 2023, pp. 47-51.
APA [1] WANG Li-ming, JIA Ya-wei, MENG Zhu, FU Li-ting, WU Jing, SONG Li-juan, & CHU Gang. (2023). Study on Thermal Stability of γ-Al2O3 Powders Modified by Samarium Doping. Rare Metals and Cemented Carbides(3), 47-51.
IEEE [1] WANG Li-ming, JIA Ya-wei, MENG Zhu, FU Li-ting, WU Jing, SONG Li-juan, and CHU Gang, "Study on Thermal Stability of γ-Al2O3 Powders Modified by Samarium Doping," Rare Metals and Cemented Carbides, no. 3, pp. 47-51, 2023. keywords: {solution combustion method;samarium doping;samarium nitrate;γ-AlO;modification;thermal stability}