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Preparation of Scandium Oxalate Powder by Liquid Precipitation Method and Its Morphology Control AITranslate

School of Metallurgy and Environment,Central South University;School of Metallurgy and Environment,Central South University;School of Metallurgy and Environment,Central South University;School of Metallurgy and Environment,Central South University;School of Metallurgy and Environment,Central South University;School of Metallurgy and Environment,Central South University
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Publisher: Editorial Office of Rare Metals and Cemented Carbides
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Abstract AITranslate

The morphology of scandium oxalate crystal was controlled b'y changing the conditions of precipitation and crystallization when adding sodium oxalate to scandium chloride solution by liquid precipitation method.The effects of solution pH,feeding method,scandium concentration,surfactant and aging time on the morphology of scandium oxalate and its mechanism were investigated.The results show that many kinds of scandium oxalate crystals,such as hexagonal sheet and thick sheet,spherical,bipyramidal and layered stacking,can be prepared by controlling different experimentaI conditions,which can promote the research and application of scandium-containing powder materials.

KeyWords AITranslate

morphology control liquid phase precipitation scandium oxalate scandium chloride sodium oxMate crystal

1刘彩云,符剑刚.钨渣中钪的萃取回收实验研究[J].稀有金属与硬质合金,2015,43(5):4-8 11. 被引量:17

2李青刚,李兆洋,孙盼,张贵清.离子交换法净化氯化钪溶液[J].东北大学学报:自然科学版,2016,37(10):1410-1414. 被引量:2

3贾志谦,刘忠洲.液相沉淀法制备纳米粒子的过程特征和原理[J].化学工程,2002,30(1):38-41. 被引量:10

4黄凯,郭学益,张多默.超细粉末湿法制备过程中粒子粒度和形貌控制的基础理论[J].粉末冶金材料科学与工程,2005(6):319-324. 被引量:17

5张军,孙聆东,廖春生,严纯华.氧化锌微晶的制备和形貌控制[J].无机化学学报,2002,18(1):72-74. 被引量:29

6赵国玺,朱步瑶.表面活性剂作用原理[J].日用化学工业信息,2003(17):16-16. 被引量:17

7彭美勋,沈湘黔,危亚辉.球形Ni(OH)2生长过程中的Ostwald熟化作用[J].电源技术,2008,32(2):106-108. 被引量:4

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1张积锴,郑诗礼,李平,杨幼明,管新地,周洁英,陈东英.复合沉淀剂制备高质量碳酸镧及氧化镧的研究[J].中国稀土学报,2022,40(4):624-632. 被引量:2

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3卢博,刘宜强,蒋威,夏侯斌,徐娜,刘欣.大颗粒氧化镧粉体制备研究进展[J].稀土,2022,43(6):119-124.

4朱群龙,汪泉,汪旭光,李瑞,涂唱畅,杨锐,朱文艳.爆轰法制备的纳米La_(2)O_(3)的表征与性能[J].高压物理学报,2023,37(4):24-33.

1吴莹莹,徐伟.Cu_2(OH)_3NO_3/Ag复合物的制备及性能研究[J].复旦学报:自然科学版,2018,57(1):1-7. 被引量:1

2郭海峰,徐振旋,江昌华,罗平英,付召福.镧掺杂对羟基磷灰石形貌与吸附性能的影响[J].萍乡学院学报,2018,35(6):45-48. 被引量:1

3彭桢,李青刚,李兆洋,张贵清,曹佐英,关文娟.用离子交换法去除含钪溶液中的杂质(英文)[J].中南大学学报:英文版,2018,25(12):2953-2961. 被引量:3

4李瑶,彭同江,孙红娟,肖青.Cu-TiO_2/白云母纳米复合材料的制备及结构、形貌和光催化性能[J].硅酸盐学报,2019,47(4):480-485. 被引量:5

5刘毓涵,姜妲,黄智恒,王宁,曲日壮,乔森荣.化学液相法制备纳米铜粉的工艺及应用进展研究[J].科技创新导报,2018,15(26):108-109. 被引量:2

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Basic Information:

DOI:

Chinese Library Classification Number:TF841.1[冶金工程—有色金属冶金]

Citation Information:

The morphology of scandium oxalate crystal was controlled b'y changing the conditions of precipitation and crystallization when adding sodium oxalate to scandium chloride solution by liquid precipitation method.The effects of solution pH,feeding method,scandium concentration,surfactant and aging time on the morphology of scandium oxalate and its mechanism were investigated.The results show that many kinds of scandium oxalate crystals,such as hexagonal sheet and thick sheet,spherical,bipyramidal and layered stacking,can be prepared by controlling different experimentaI conditions,which can promote the research and application of scandium-containing powder materials.

quote

GB/T 7714-2015 [1] LI Qing-gang, PENG Zhen, ZHANG Gui-qing, et al. Preparation of Scandium Oxalate Powder by Liquid Precipitation Method and Its Morphology Control[J]. Rare Metals and Cemented Carbides, 2019(1): 11-15.
MLA [1] LI Qing-gang, et al., "Preparation of Scandium Oxalate Powder by Liquid Precipitation Method and Its Morphology Control." Rare Metals and Cemented Carbides, no. 1, 2019, pp. 11-15.
APA [1] LI Qing-gang, PENG Zhen, ZHANG Gui-qing, CAO Zuo-ying, ZENG Li, & GUAN Wen-juan. (2019). Preparation of Scandium Oxalate Powder by Liquid Precipitation Method and Its Morphology Control. Rare Metals and Cemented Carbides(1), 11-15.
IEEE [1] LI Qing-gang, PENG Zhen, ZHANG Gui-qing, CAO Zuo-ying, ZENG Li, and GUAN Wen-juan, "Preparation of Scandium Oxalate Powder by Liquid Precipitation Method and Its Morphology Control," Rare Metals and Cemented Carbides, no. 1, pp. 11-15, 2019. keywords: {morphology control;liquid phase precipitation;scandium oxalate;scandium chloride;sodium oxMate;crystal}