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Study on Preparation of High-purity Platinum AITranslate

Kunming Institute of Precious Metals;Kunming Institute of Precious Metals;Kunming Institute of Precious Metals;Kunming Institute of Precious Metals;Kunming Institute of Precious Metals;Kunming Institute of Precious Metals
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Publisher: Editorial Office of Rare Metals and Cemented Carbides
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Abstract AITranslate

High-purity platinum was prepared by the combination process of dissolution of crude platinum with aqua regia-oxidation and carrier hydrolysis-ion exchange-NH4 Cl precipitation,and the effects of impu- rity elements removal in each process step were studied. The experimental results show that platinum can be effectively separated from other precious metals and base metals by dissolution of crude platinum with aqua regia, and then oxidation and carrier hydrolysis,ion exchange and precipitation of Pt-containing solution. The obtained purified (NH4)2 PtCl6 precursor was calcined and washed,and Pt powder was prepared. Based on GDMS analysis,the impurity content in Pt powder is less than 3 ×10^-6 ,and the purity of platinum is more than 99. 999%.

KeyWords AITranslate

high-purity platinum dissolution with aqua regia carrier hydrolysis ion exchange NHL Cl precipitation

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Basic Information:

DOI:

Chinese Library Classification Number:TF114[冶金工程—冶金物理化学]

Citation Information:

High-purity platinum was prepared by the combination process of dissolution of crude platinum with aqua regia-oxidation and carrier hydrolysis-ion exchange-NH4 Cl precipitation,and the effects of impu- rity elements removal in each process step were studied. The experimental results show that platinum can be effectively separated from other precious metals and base metals by dissolution of crude platinum with aqua regia, and then oxidation and carrier hydrolysis,ion exchange and precipitation of Pt-containing solution. The obtained purified (NH4)2 PtCl6 precursor was calcined and washed,and Pt powder was prepared. Based on GDMS analysis,the impurity content in Pt powder is less than 3 ×10^-6 ,and the purity of platinum is more than 99. 999%.

quote

GB/T 7714-2015 [1] YANG Hai-qiong, ZHAO Jia-chun, CHEN Jia-lin, et al. Study on Preparation of High-purity Platinum[J]. Rare Metals and Cemented Carbides, 2018(2): 64-67.
MLA [1] YANG Hai-qiong, et al., "Study on Preparation of High-purity Platinum." Rare Metals and Cemented Carbides, no. 2, 2018, pp. 64-67.
APA [1] YANG Hai-qiong, ZHAO Jia-chun, CHEN Jia-lin, LI Bo-jie, WANG Ying-wu, & DONG Hai-gang. (2018). Study on Preparation of High-purity Platinum. Rare Metals and Cemented Carbides(2), 64-67.
IEEE [1] YANG Hai-qiong, ZHAO Jia-chun, CHEN Jia-lin, LI Bo-jie, WANG Ying-wu, and DONG Hai-gang, "Study on Preparation of High-purity Platinum," Rare Metals and Cemented Carbides, no. 2, pp. 64-67, 2018. keywords: {high-purity platinum;dissolution with aqua regia;carrier hydrolysis;ion exchange;NHL Cl precipitation}