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Research on Micromorphology and Performance of TiAlN Coating and TiAlSiN Coating on Zirconium Alloy Surface AITranslate

School of Mechanical Engineering, Nanhua University;School of Mechanical Engineering, Nanhua University;School of Mechanical Engineering, Nanhua University;School of Mechanical Engineering, Nanhua University;School of Mechanical Engineering, Nanhua University
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Publisher: Editorial Office of Rare Metals and Cemented Carbides
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Abstract AITranslate

TiAlSiN coating and TiAlN coating were deposited on Zr-4 alloy surface by multi-arc ion plating,respectively.Surface micromorphology of the coatings were observed by scanning electron microscope.Statistics and analysis of the large particle distribution of the coatings were carried out by ImageJ.The phase composition of the coatings was analyzed by X-ray diffractometer.The mechanical properties of the coatings were tested by an automatic scratch tester.And the samples were subjected to 800℃ high temperature oxidation resistance test in a high temperature heat treatment furnace.The results show that the amount of large particles on the surface of TiAlSiN coating is less than that of TiAlN coating.Both TiAlSiN coating and TiAlN coating have Ti2N phase and Ti3AlN phase.In addition,TiAlSiN coating also has AlN phase and Si3N4 amorphous phase.Because the addition of Si elements leads to residual stress,TiAlSiN coating has lower coating/substrate adhesion strength than TiAlN coating.Oxidation weight gain of TiAlSiN coating sample is far lower than that of TiAlN coating sample.

KeyWords AITranslate

Zr-4 alloy TiAlSiN coating TiAlN coating multi-arc ion plating high temperature oxidation resistance coating/substrate adhesion strength

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Basic Information:

DOI:

Chinese Library Classification Number:TG146.414[金属学及工艺—金属材料]

Citation Information:

TiAlSiN coating and TiAlN coating were deposited on Zr-4 alloy surface by multi-arc ion plating,respectively.Surface micromorphology of the coatings were observed by scanning electron microscope.Statistics and analysis of the large particle distribution of the coatings were carried out by ImageJ.The phase composition of the coatings was analyzed by X-ray diffractometer.The mechanical properties of the coatings were tested by an automatic scratch tester.And the samples were subjected to 800℃ high temperature oxidation resistance test in a high temperature heat treatment furnace.The results show that the amount of large particles on the surface of TiAlSiN coating is less than that of TiAlN coating.Both TiAlSiN coating and TiAlN coating have Ti2N phase and Ti3AlN phase.In addition,TiAlSiN coating also has AlN phase and Si3N4 amorphous phase.Because the addition of Si elements leads to residual stress,TiAlSiN coating has lower coating/substrate adhesion strength than TiAlN coating.Oxidation weight gain of TiAlSiN coating sample is far lower than that of TiAlN coating sample.

quote

GB/T 7714-2015 [1] ZHOU Jun, FAN Xiang-fang, FENG Zhen-dong, et al. Research on Micromorphology and Performance of TiAlN Coating and TiAlSiN Coating on Zirconium Alloy Surface[J]. Rare Metals and Cemented Carbides, 2017(6): 66-70.
MLA [1] ZHOU Jun, et al., "Research on Micromorphology and Performance of TiAlN Coating and TiAlSiN Coating on Zirconium Alloy Surface." Rare Metals and Cemented Carbides, no. 6, 2017, pp. 66-70.
APA [1] ZHOU Jun, FAN Xiang-fang, FENG Zhen-dong, HU Ru-qian, & LI Huai-lin. (2017). Research on Micromorphology and Performance of TiAlN Coating and TiAlSiN Coating on Zirconium Alloy Surface. Rare Metals and Cemented Carbides(6), 66-70.
IEEE [1] ZHOU Jun, FAN Xiang-fang, FENG Zhen-dong, HU Ru-qian, and LI Huai-lin, "Research on Micromorphology and Performance of TiAlN Coating and TiAlSiN Coating on Zirconium Alloy Surface," Rare Metals and Cemented Carbides, no. 6, pp. 66-70, 2017. keywords: {Zr-4 alloy;TiAlSiN coating;TiAlN coating;multi-arc ion plating;high temperature oxidation resistance;coating/substrate adhesion strength}