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Study on Preparation Process of Yttrium-Stabilized Nano-Zirconia by Hydrothermal Hydrolysis AITranslate

Chalco Guangxi Non-Ferrous Rare Earth Development Co.,Ltd.;Chalco Guangxi Non-Ferrous Rare Earth Development Co.,Ltd.;Chalco Guangxi Non-Ferrous Rare Earth Development Co.,Ltd.;Chalco Guangxi Non-Ferrous Rare Earth Development Co.,Ltd.;Chalco Guangxi Non-Ferrous Rare Earth Development Co.,Ltd.
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Publisher: Editorial Office of Rare Metals and Cemented Carbides
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Abstract AITranslate

Yttrium-stabilized zirconia(YSZ)was prepared by hydrothermal hydrolysis using zirconium oxychloride,yttrium chloride,and ammonia as raw materials and polyethylene glycol as a dispersant.The effects of zirconium ion concentration,reaction temperature,yttrium doping amount,dispersant addition,and calcination temperature on the morphology,dispersity,particle size,and crystal form of the zirconia products were systematically studied.The results show that under the conditions of zirconium ion concentration of 0.8 mol/L,reaction temperature of 180℃,yttrium doping amount of 3%(molar fraction),dispersant addition of 2%(mass fraction),and calcination temperature of 1000℃,yttrium-stabilized nano-zirconia powders with good dispersity,uniform particle size distribution and spherical-like shape could be obtained.

KeyWords AITranslate

yttrium-stabilized nano-zirconia hydrothermal hydrolysis zirconium oxychloride ammonia process condition

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DOI:

Chinese Library Classification Number:TQ134.12[化学工程—无机化工]

Citation Information:

Yttrium-stabilized zirconia(YSZ)was prepared by hydrothermal hydrolysis using zirconium oxychloride,yttrium chloride,and ammonia as raw materials and polyethylene glycol as a dispersant.The effects of zirconium ion concentration,reaction temperature,yttrium doping amount,dispersant addition,and calcination temperature on the morphology,dispersity,particle size,and crystal form of the zirconia products were systematically studied.The results show that under the conditions of zirconium ion concentration of 0.8 mol/L,reaction temperature of 180℃,yttrium doping amount of 3%(molar fraction),dispersant addition of 2%(mass fraction),and calcination temperature of 1000℃,yttrium-stabilized nano-zirconia powders with good dispersity,uniform particle size distribution and spherical-like shape could be obtained.

quote

GB/T 7714-2015 [1] TAN Hai-xiang, QIN Wen-zhong, WEI Shi-qiang, et al. Study on Preparation Process of Yttrium-Stabilized Nano-Zirconia by Hydrothermal Hydrolysis[J]. Rare Metals and Cemented Carbides, 2023(3): 77-81.
MLA [1] TAN Hai-xiang, et al., "Study on Preparation Process of Yttrium-Stabilized Nano-Zirconia by Hydrothermal Hydrolysis." Rare Metals and Cemented Carbides, no. 3, 2023, pp. 77-81.
APA [1] TAN Hai-xiang, QIN Wen-zhong, WEI Shi-qiang, GAN Pei-yuan, & HUANG Yu-feng. (2023). Study on Preparation Process of Yttrium-Stabilized Nano-Zirconia by Hydrothermal Hydrolysis. Rare Metals and Cemented Carbides(3), 77-81.
IEEE [1] TAN Hai-xiang, QIN Wen-zhong, WEI Shi-qiang, GAN Pei-yuan, and HUANG Yu-feng, "Study on Preparation Process of Yttrium-Stabilized Nano-Zirconia by Hydrothermal Hydrolysis," Rare Metals and Cemented Carbides, no. 3, pp. 77-81, 2023. keywords: {yttrium-stabilized nano-zirconia;hydrothermal hydrolysis;zirconium oxychloride;ammonia;process condition}