Gaseous Detonation Synthesis and Characterization of TiO_2-SiO_2 Nanometer Composite Oxide AITranslate
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TiO2-SiO2 nanometer composite oxide was prepared by gaseous detonation with H2 and O2 premixed gas as the explosion source,and TiCl4 and SiCl4 as the precursor.The influence of precursor Ti/Si ratio on the detonation product was investigated.Crystal structure,morphology and chemical composition of the detonation product were analyzed by XRD,TEM and FTIR.The resluts show that TiO2 is a mixture crystal of ruble and anatase in TiO2-SiO2 nanometer composite oxide,and SiO2 is amorphous.There is Ti—O—Si bond in TiO2-SiO2 nanometer composite oxide particles.amorphous adheres to the exterior of the crystalline TiO2 in the obtained TiO2-SiO2 composite structure.And the composite structure changes with precursor Ti/Si ratio.
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4胡彦杰,李春忠,丛德滋,姜海波,赵尹.氢氧焰燃烧合成核壳结构纳米TiO_2／SiO_2复合颗粒及机理分析[J].无机材料学报,2007,22(2):205-208. 被引量：5
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Chinese Library Classification Number:O383[理学—流体力学]
Citation Information:
TiO2-SiO2 nanometer composite oxide was prepared by gaseous detonation with H2 and O2 premixed gas as the explosion source,and TiCl4 and SiCl4 as the precursor.The influence of precursor Ti/Si ratio on the detonation product was investigated.Crystal structure,morphology and chemical composition of the detonation product were analyzed by XRD,TEM and FTIR.The resluts show that TiO2 is a mixture crystal of ruble and anatase in TiO2-SiO2 nanometer composite oxide,and SiO2 is amorphous.There is Ti—O—Si bond in TiO2-SiO2 nanometer composite oxide particles.amorphous adheres to the exterior of the crystalline TiO2 in the obtained TiO2-SiO2 composite structure.And the composite structure changes with precursor Ti/Si ratio.
quote
| GB/T 7714-2015 | [1] KONG Xiang-qing, ZHU Kai-ze, GAO Hua-dong, et al. Gaseous Detonation Synthesis and Characterization of TiO_2-SiO_2 Nanometer Composite Oxide[J]. Rare Metals and Cemented Carbides, 2018(1): 44-48. |
| MLA | [1] KONG Xiang-qing, et al., "Gaseous Detonation Synthesis and Characterization of TiO_2-SiO_2 Nanometer Composite Oxide." Rare Metals and Cemented Carbides, no. 1, 2018, pp. 44-48. |
| APA | [1] KONG Xiang-qing, ZHU Kai-ze, GAO Hua-dong, & QU Yan-dong. (2018). Gaseous Detonation Synthesis and Characterization of TiO_2-SiO_2 Nanometer Composite Oxide. Rare Metals and Cemented Carbides(1), 44-48. |
| IEEE | [1] KONG Xiang-qing, ZHU Kai-ze, GAO Hua-dong, and QU Yan-dong, "Gaseous Detonation Synthesis and Characterization of TiO_2-SiO_2 Nanometer Composite Oxide," Rare Metals and Cemented Carbides, no. 1, pp. 44-48, 2018. keywords: {TiO2-SiO2 composite oxide;nanometer powder;gaseous detonation;precursor Ti/Si ratio} |