The Influence of Monomer Concentration on Gelation and Property of Porous Titanium AITranslate
Abstract AITranslate
Porous titanium compacts were prepared by gelatining solidification and vacuum sintering techThe influence of monomer concentration on gelatining solidification,microstructure and properties of sintered compact of porous titanium were analyzed by scanning electron microscope (SEM), differential scanning calorimeter (DSC) and mechanical testing machine. The results showed that the role of dispersant citrate ammonium was apparent when the pH values of slurry were in the range from 7 to 9. When the monomer content,the added volume for the initiator and the ammonium are 20% 6mmol/L and 0.1 mL, respectively,the gelatin time is 68 rain at 45℃ reaction temperature. The bending strength of green compact with the monomer content of 15%,29% and 25% are about 15.2 MPa,20.6 MPa and 24.1 MPa,respectively. The green compact is sintered at 1 100℃ for 2 h,and the open-porosity ofsintered porous tita- nium is 39.5%.
KeyWords AITranslate
1Fujibayashi S, Neo M, Kim H M, et al. Osteoinduction of porous bioactive titanium metal[J]. Biomaterials, 2004, 25(3) :443-450.
2李伯琼,王德庆,陆兴.粉末冶金多孔钛的研究[J].大连铁道学院学报,2004,25(1):74-78. 被引量:19
3姜淑文,齐民.生物医用多孔金属材料的研究进展[J].材料科学与工程,2002,20(4):597-600. 被引量:19
4Nomura N, Kohama T, Oh I H, et al. Mechanical properties of porous Ti-15Mo-SZr-3Al compacts prepared by powder sintering[J]. Materials Science and Engineering C, 2005,25 (3): 330-335.
5Wen C E, Mabuchi M, Yamada Y, et al. Processing of biocompatible porous Ti and Mg[J]. Scripta Materialia, 2001,45(10):1 147-1 153.
6An Y g,Oh N H,Chun Y W,et al. Mechanical properties of environmental electro discharge sintered porous Ti implants[J]. Materials Letters, 2005,59 (17) : 2 178- 2 182.
7Omatete O O, Janney M A, Strehlow R A. Gelcasting--A new ceramic forming process[J]. American Ceramic Society Bulletin, 1991,70(10) : 1 641-1 649.
8Erk K A, Dunand D C, Shull K R. Titanium with controilabie pore fractions by thermoreversible gelcasting of TiHz[J]. Acta Materialia,2008,56(18):5 147-5 157.
9李艳,郭志猛,郝俊杰,任淑彬.凝胶注模成型制备医用多孔钛植入材料及其性能[J].功能材料,2007,38(A05):1758-1761. 被引量:1
10Ortega F S, Sepulveda P, Pandolfelli V C. Monomer systems for the geleasting of foams[J]. Journal of the European Ceramic Society, 2002, 22 (9 - 10 ) : 1 395 - 1 401.
1张二林,王晓燕,憨勇.医用多孔Ti及钛合金的国内研究现状[J].金属学报,2017,53(12):1555-1567. 被引量:12
1吴姗姗,刘继光,李慕勤,张二林,姚海涛,迟艳侠,李艳芳.Ti-Cu合金微弧氧化种植体的动物体内骨结合行为[J].中国体视学与图像分析,2018,23(4):359-368.
2田银宝,申俊琦,胡绳荪,勾健.丝材+电弧增材制造钛/铝异种金属反应层的研究[J].金属学报,2019,55(11):1407-1416. 被引量:12
3王耀奇,王晓华,王哲磊,任学平,侯红亮.泡沫钛制备及力学性能评价研究[J].稀有金属材料与工程,2020,49(3):1051-1057. 被引量:2
4张聪,贾德君,李范春,徐一通,张源.面向3D打印的钛合金点阵接骨板设计及其仿真[J].上海交通大学学报,2021,55(2):170-178. 被引量:1
5陈海军,师启华,尹丹凤,高雷章.宇航级钒铝合金脱氧技术研究[J].钢铁钒钛,2020,41(6):16-20.
6胡勇,李申申,吴栋,李英新,康文江,张昊,张会莹.聚多巴胺接枝纳米氧化锌复合涂层对TC4合金表面修饰的影响[J].稀有金属材料与工程,2021,50(8):2876-2882.
7王浩,卢明亮,万贺利.提钒工艺研究现状及进展[J].河北冶金,2021(12):6-9. 被引量:2
8张美丽,叱小彤,周春生,刘彦峰,方琛,郑郭刚.多孔Ti-Nb合金材料的制备与性能研究[J].钢铁钒钛,2021,42(6):84-89.
9麦萍.硬脂酸添加量对多孔Ti-5Cu合金微观结构及性能的影响[J].热加工工艺,2022,51(24):25-29.
10张东阳,张钧,李述军,任德春,马英杰,杨锐.热处理对选区激光熔化Ti55531合金多孔材料力学性能的影响[J].金属学报,2023,59(5):647-656. 被引量:1
1肖靖,张剑德.钼酸盐复配缓蚀剂对铜的缓蚀性能研究[J].硅谷,2011,4(23):105-106. 被引量:5
2魏然,邵慧萍,林涛,郭志猛.孔隙率对钛合金生物医用材料耐蚀性的影响[J].功能材料,2012,43(B11):178-181. 被引量:2
3黎春阳,任瑞铭,董洪亮.Al_2O_3基陶瓷基片的制备及其性能[J].大连交通大学学报,2008,29(3):54-57. 被引量:2
4李艳,郭志猛,郝俊杰,高玉喜.工艺参数对凝胶注模成型不锈钢坯体强度和烧结密度的影响[J].中国学术期刊文摘,2008,14(12):94-94.
5杜景红,宋宁,史庆南,孙加林.凝胶注模成形技术的研究与发展[J].陶瓷,2006(1):19-23. 被引量:12
6徐惠,王新颖,刘小育.聚苯胺/银复合薄膜的制备及其耐蚀性能[J].材料保护,2010,43(10):11-13. 被引量:4
7杨来侠,郭丽萍,韩香广.凝胶注模氧化铝陶瓷浆料充型能力研究[J].铸造技术,2013,34(5):587-589. 被引量:3
8欧阳飞,徐元,徐小平,皇甫琴,张湘丁,杨园,刘建东.焦磷酸盐镀铜溶液中柠檬酸铵含量的测定[J].电镀与精饰,2016,38(12):42-43. 被引量:2
9王小锋,王日初,彭超群,李婷婷,罗玉林,王超,刘兵.凝胶注模成型技术的研究与进展[J].中国有色金属学报,2010,20(3):496-509. 被引量:51
10刘海鹏,张志桐,王心悦,孟庆波,李运刚,杨海丽.柠檬酸铵浓度对脉冲电镀Ni-Cr-Mo合金镀层的影响[J].表面技术,2016,45(11):81-86. 被引量:5
Basic Information:
DOI:
Chinese Library Classification Number:TG146.23[金属学及工艺—金属材料]
Citation Information:
Porous titanium compacts were prepared by gelatining solidification and vacuum sintering techThe influence of monomer concentration on gelatining solidification,microstructure and properties of sintered compact of porous titanium were analyzed by scanning electron microscope (SEM), differential scanning calorimeter (DSC) and mechanical testing machine. The results showed that the role of dispersant citrate ammonium was apparent when the pH values of slurry were in the range from 7 to 9. When the monomer content,the added volume for the initiator and the ammonium are 20% 6mmol/L and 0.1 mL, respectively,the gelatin time is 68 rain at 45℃ reaction temperature. The bending strength of green compact with the monomer content of 15%,29% and 25% are about 15.2 MPa,20.6 MPa and 24.1 MPa,respectively. The green compact is sintered at 1 100℃ for 2 h,and the open-porosity ofsintered porous tita- nium is 39.5%.
quote
| GB/T 7714-2015 | [1] HU Hai-bo, FU Shang, WANG Jie-en, et al. The Influence of Monomer Concentration on Gelation and Property of Porous Titanium[J]. Rare Metals and Cemented Carbides, 2011(4): 31-36. |
| MLA | [1] HU Hai-bo, et al., "The Influence of Monomer Concentration on Gelation and Property of Porous Titanium." Rare Metals and Cemented Carbides, no. 4, 2011, pp. 31-36. |
| APA | [1] HU Hai-bo, FU Shang, WANG Jie-en, LIU Hui-qun, & SUN Wu-ling. (2011). The Influence of Monomer Concentration on Gelation and Property of Porous Titanium. Rare Metals and Cemented Carbides(4), 31-36. |
| IEEE | [1] HU Hai-bo, FU Shang, WANG Jie-en, LIU Hui-qun, and SUN Wu-ling, "The Influence of Monomer Concentration on Gelation and Property of Porous Titanium," Rare Metals and Cemented Carbides, no. 4, pp. 31-36, 2011. keywords: {porous titanium;monomer concentration;gelatining;gelcasting;vacuum sintering} |
