Hydrothermal Synthesis and Characterization of β-Ni(OH)_2 Petal-shaped Sphere and Nanoplate AITranslate
Abstract AITranslate
β-Ni（OH）2 petal-shaped sphere and nanoplate were synthesized by hydrothermal method with strong ammonia as the precipitator and nickel nitrate as the nickel source.The above synthesis method is simple and easy to operate.The phase structure and morphology were analyzed using XRD and SEM.The results show that under the same pH value and reaction time,low temperature is good for the synthesis of β-Ni（OH）2 petal-shaped sphere,while high temperature is good for the synthesis of β-Ni（OH）2 nanoplate.β-Ni（OH）2 petal-shaped sphere and nanoplate are obtained at 180 ℃ and 240 ℃,respectively,both by reacting at pH 9.0 for 48.0 h.Based on the effects of hydrothermal synthesis conditions on morphology of the sample,the formation mechanism of β-Ni（OH）2 petal-shaped sphere and nanoplate is discussed.
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Basic Information:
DOI：
Chinese Library Classification Number:TQ138.13[化学工程—无机化工]
Citation Information:
β-Ni（OH）2 petal-shaped sphere and nanoplate were synthesized by hydrothermal method with strong ammonia as the precipitator and nickel nitrate as the nickel source.The above synthesis method is simple and easy to operate.The phase structure and morphology were analyzed using XRD and SEM.The results show that under the same pH value and reaction time,low temperature is good for the synthesis of β-Ni（OH）2 petal-shaped sphere,while high temperature is good for the synthesis of β-Ni（OH）2 nanoplate.β-Ni（OH）2 petal-shaped sphere and nanoplate are obtained at 180 ℃ and 240 ℃,respectively,both by reacting at pH 9.0 for 48.0 h.Based on the effects of hydrothermal synthesis conditions on morphology of the sample,the formation mechanism of β-Ni（OH）2 petal-shaped sphere and nanoplate is discussed.
quote
| GB/T 7714-2015 | [1] FU Xiao-ming, LIU Zhao-wen. Hydrothermal Synthesis and Characterization of β-Ni(OH)_2 Petal-shaped Sphere and Nanoplate[J]. Rare Metals and Cemented Carbides, 2012(2): 29-32. |
| MLA | [1] FU Xiao-ming, and LIU Zhao-wen. "Hydrothermal Synthesis and Characterization of β-Ni(OH)_2 Petal-shaped Sphere and Nanoplate." Rare Metals and Cemented Carbides, no. 2, 2012, pp. 29-32. |
| APA | [1] FU Xiao-ming, & LIU Zhao-wen. (2012). Hydrothermal Synthesis and Characterization of β-Ni(OH)_2 Petal-shaped Sphere and Nanoplate. Rare Metals and Cemented Carbides(2), 29-32. |
| IEEE | [1] FU Xiao-ming and LIU Zhao-wen, "Hydrothermal Synthesis and Characterization of β-Ni(OH)_2 Petal-shaped Sphere and Nanoplate," Rare Metals and Cemented Carbides, no. 2, pp. 29-32, 2012. keywords: {β-Ni（OH）2 petal-shaped sphere;β-Ni（OH）2 nanoplate;nickel nitrate;strong ammonia;hydrothermal method} |