Research on Determination of Trace Nitrate in Rare Earth Hydroxides by Spectrophotometry AITranslate
Abstract AITranslate
Trace nitrate in rare earth hydroxides was determined by spectrophotometry with indigo carmine as the chromogenic reagent.The influence was investigated of different factors on nitrate determination,and the optimum analytical conditions were determined.When nitrate concentration is 0~1.0μg/mL,there is a linear relationship between color fading degree and nitrate content following Beer's law.The relative standard deviation of the measured nitrate content is 2.41%,and the standard addition recovery is 97.6%~101.3%.This method to determine trace nitrate in rare earth hydroxides is characterized by simple operation and accurate test results.
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1Kazuaki Ito,Yohichi Takayama,Nobuyuki Makabe,Ryo Mitsui,Takeshi Hirokawa.Ion chromatography for determination of nitrite and nitrate in seawater using monolithic ODS columns[J]. Journal of Chromatography A . 2005 (1)
2Possible role of nitrate/nitrite redox cycles in catalytic and selective sulfoxidation reaction[J]. Applied Catalysis A, General . 2003 (2)
1孟祖超,李成希,郭敏,杨义磊,孟昱婷,毛云霞.Cu-Ag/石墨烯修饰电极的制备及其对亚硝酸盐的测定[J].分析试验室,2016,35(5):560-564. 被引量：4
2邱立萍,吕瑞亮.离子色谱法测定墓葬土壤中5种阴离子[J].理化检验：化学分册,2018,54(8):963-966. 被引量：4
3龙尚俊,刘云贵,龙安禄,朱绍严,周元敬.分光光度法测定肥料中硝酸根[J].贵州科学,2020,38(5):93-96.
1习霞,明亮.线性扫描伏安法测定腌菜中亚硝酸盐含量[J].中国调味品,2018,43(7):139-142. 被引量：3
2刘晓鹏,贺全国,刘军,李广利,梁静,邓培红.石墨烯复合材料在电化学检测食品中亚硝酸盐的研究进展[J].食品科学,2018,39(23):337-345. 被引量：4
3李吉庆,李仁勇,赵全升,王玲.离子色谱法测定左乙拉西坦中N-甲基苄胺[J].分析试验室,2019,38(7):863-866. 被引量：4
4罗婷容,石维平,刘冰倩,聂方钦,邓雪锦,刘跃芝.无标记均相电化学传感器快速测定水体中亚硝酸根[J].分析试验室,2019,0(9):1035-1038. 被引量：3
5董莉丽.植被恢复对土壤水溶性阴离子浓度的影响[J].河南科学,2020,38(5):721-727. 被引量：2
6甘欣欣.离子色谱及其样品前处理技术在文物保护中的应用和进展[J].文物鉴定与鉴赏,2021(4):51-54. 被引量：1
7邱立萍,刘丽娜,张晓凤.离子色谱法测定墓葬壁画土壤中4种阴离子[J].应用化工,2023,52(5):1602-1605.
8杜维莎,景博文,付菲,李华,夏寅,周萍.离子色谱法快速测定秦陵土遗址中无机阴、阳离子含量[J].中国无机分析化学,2023,13(10):1097-1103.
1冉广芬,陈玉锋,马海洲,许建新,高东林,孟庆芬.分光光度法测定含氯矿物中微量硝酸根[J].无机盐工业,2006,38(10):57-59. 被引量：2
2李国斌,杨亚玲,杨万明.黄磷中硝酸根测定方法的研究[J].云南化工,2000,27(2):37-38. 被引量：4
3唐次来,张增强,张永涛,王学友.紫外分光光度法直接测定硝酸根含量的波长优化选择[J].理化检验：化学分册,2008,44(7):634-636. 被引量：5
4刘琼,杨刚宾,薛冬,张莹莹.催化光度法测定痕量亚硝酸根[J].河南理工大学学报：自然科学版,2013,32(6):756-759. 被引量：1
5王谦,李同真,刘传玉.硝酸根、亚硝酸根同时存在下的硝酸根含量测定[J].化学与粘合,1995,17(2):87-88.
6刘晓庚,张国岩,蒋帅.甲基橙褪色光度法快速测定食品中亚硝酸根含量[J].理化检验：化学分册,2005,41(12):925-927. 被引量：5
7郑肇生,吴和舟,曾文忠.溴酸钾氧化茜素绿催化光度法测定痕量亚硝酸根[J].分析化学,1993,21(6):669-671. 被引量：33
8白林山,张艳,张建锋,徐雁玲.靛蓝二磺酸钠催化光度法测定水中痕量亚硝酸根[J].华东冶金学院学报,2000,17(1):24-26. 被引量：3
9李建平,段德良.硝酸根离子选择电极—流动注射方法测定NO^—3[J].桂林冶金地质学院学报,1994,14(4):424-427.
10丁明星.使胶状稀土氢氧化物成大颗粒沉淀与除去杂质钡、钙、镁的研究[J].西昌学院学报：社会科学版,1997,0(1):30-35.
Basic Information:
DOI：
Chinese Library Classification Number:TQ133.3[化学工程—无机化工];O657.3[理学—分析化学]
Citation Information:
Trace nitrate in rare earth hydroxides was determined by spectrophotometry with indigo carmine as the chromogenic reagent.The influence was investigated of different factors on nitrate determination,and the optimum analytical conditions were determined.When nitrate concentration is 0~1.0μg/mL,there is a linear relationship between color fading degree and nitrate content following Beer's law.The relative standard deviation of the measured nitrate content is 2.41%,and the standard addition recovery is 97.6%~101.3%.This method to determine trace nitrate in rare earth hydroxides is characterized by simple operation and accurate test results.
quote
| GB/T 7714-2015 | [1] YI Shi, LIU Rong-li, ZOU Long. Research on Determination of Trace Nitrate in Rare Earth Hydroxides by Spectrophotometry[J]. Rare Metals and Cemented Carbides, 2015(5): 72-74. |
| MLA | [1] YI Shi, et al., "Research on Determination of Trace Nitrate in Rare Earth Hydroxides by Spectrophotometry." Rare Metals and Cemented Carbides, no. 5, 2015, pp. 72-74. |
| APA | [1] YI Shi, LIU Rong-li, & ZOU Long. (2015). Research on Determination of Trace Nitrate in Rare Earth Hydroxides by Spectrophotometry. Rare Metals and Cemented Carbides(5), 72-74. |
| IEEE | [1] YI Shi, LIU Rong-li, and ZOU Long, "Research on Determination of Trace Nitrate in Rare Earth Hydroxides by Spectrophotometry," Rare Metals and Cemented Carbides, no. 5, pp. 72-74, 2015. keywords: {rare earth hydroxide;nitrate determination;spectrophotometry;indigo carmine} |