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Research on the Thermal Decomposition of CoC_2O_4·2H_2O in the Argon Gas AITranslate

Suqian College 3 Department;Suqian College 3 Department;Suqian College 3 Department
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Publisher: Editorial Office of Rare Metals and Cemented Carbides
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Abstract AITranslate

Analysis is made on the thermal decomposition of CoC2O4 · 2H2O in the argon gas by TG-DSC and laser granulometer. The results showed that the thermal decomposition was done in two stages. First, the crystal water in CoC2O4 · 2H2O was lost at 150~275 ℃. Then,CoC2O4 was pyrolyzed into cobalt pow- der at 300~450℃. At 328.0~347.7℃ ,the biggest particle size change is found in the product,while at 347.7~500℃ ,the product particle size change is less. And between room temperature and 226.2 ℃ ,and at 226.2~328.0℃ ,the particle size change is not obvious. Therefore, the thermal decomposition condition of CoC2O4 · 2H2O in the argon gas can be controlled in stages in order to prepare cobalt powder of different particle sizes.

KeyWords AITranslate

CoC2O4 · 2H2O thermal decomposition TG-DSC particle size distribution

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DOI:

Chinese Library Classification Number:TF803.123[冶金工程—有色金属冶金]

Citation Information:

Analysis is made on the thermal decomposition of CoC2O4 · 2H2O in the argon gas by TG-DSC and laser granulometer. The results showed that the thermal decomposition was done in two stages. First, the crystal water in CoC2O4 · 2H2O was lost at 150~275 ℃. Then,CoC2O4 was pyrolyzed into cobalt pow- der at 300~450℃. At 328.0~347.7℃ ,the biggest particle size change is found in the product,while at 347.7~500℃ ,the product particle size change is less. And between room temperature and 226.2 ℃ ,and at 226.2~328.0℃ ,the particle size change is not obvious. Therefore, the thermal decomposition condition of CoC2O4 · 2H2O in the argon gas can be controlled in stages in order to prepare cobalt powder of different particle sizes.

quote

GB/T 7714-2015 [1] FU Xiao-ming, YANG Zai-zhi, LIU Zhao-wen. Research on the Thermal Decomposition of CoC_2O_4·2H_2O in the Argon Gas[J]. Rare Metals and Cemented Carbides, 2011(4): 8-12.
MLA [1] FU Xiao-ming, et al., "Research on the Thermal Decomposition of CoC_2O_4·2H_2O in the Argon Gas." Rare Metals and Cemented Carbides, no. 4, 2011, pp. 8-12.
APA [1] FU Xiao-ming, YANG Zai-zhi, & LIU Zhao-wen. (2011). Research on the Thermal Decomposition of CoC_2O_4·2H_2O in the Argon Gas. Rare Metals and Cemented Carbides(4), 8-12.
IEEE [1] FU Xiao-ming, YANG Zai-zhi, and LIU Zhao-wen, "Research on the Thermal Decomposition of CoC_2O_4·2H_2O in the Argon Gas," Rare Metals and Cemented Carbides, no. 4, pp. 8-12, 2011. keywords: {CoC2O4 · 2H2O thermal decomposition ;TG-DSC; particle size distribution}