Experimental Research on Preparation of Zirconium Oxychloride from Fused Zirconia AITranslate
Abstract AITranslate
Zirconium oxychloride was prepared from fused zirconia with the acid-alkali method. The effects were studied of fused zirconia-sodium hydroxide proportion, alkali fusion temperature and alkali fusion time on the conversion rate of zirconium during alkali fusion. The results show that the optimum conditions for alkali fusion are as follows ： mass ratio of fused zirconia to sodium hydroxide 1 ： 1,alkali fusion temperature 790 ℃ and alkali fusion time 1.5 h. Zirconium oxychloride prepared with the above method has a main grade of 36. 25%, Zr recovery rate reaches 91% ,Na2SiO3consumption reduces by more than 98% ,and alkali consumption can be reduced by 52%.
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1罗方承,吕文广,罗新文.硫酸锆、碳酸锆的性质、应用及生产技术综述[J].稀有金属,2003,27(1):53-56. 被引量：8
2林振汉.中国锆化学制品的发展及前景[J].稀有金属快报,2007,26(1):17-21. 被引量：15
3罗方承,陈忠锡,孙小龙,谌美玲.MIBK双溶剂萃取法制备原子能级氧化锆和氧化铪的工艺设计[J].稀有金属快报,2007,26(1):89-92. 被引量：13
4张建东,陈伟东,吴延科,徐志高,王力军.氯氧化锆生产中废碱水和锆硅渣回收利用研究进展[J].稀有金属,2010,34(6):936-944. 被引量：9
5宋作人,徐宝奎,李福山.中国电熔氧化锆的生产和市场展望[J].耐火材料,2007,41(4):293-297. 被引量：4
6罗方承,吴传官,杨勇,陈忠锡,李泉华,廖文中,吕文广.10000吨氧氯化锆生产工艺的改进研究和经济效益分析[J].矿产与地质,2001,15(z1):535-539. 被引量：5
7刘长河,王泽斌,王力军,熊炳昆.碱熔法氯化法制备氯氧化锆的技术经济比较[J].稀有金属快报,2007,26(1):97-99. 被引量：11
1张铭媛,康娟雪,普婧,黄秀兰,段利平,彭金辉,陈菓.氧化锆制备技术的研究现状与进展[J].矿冶,2019,28(3):75-79. 被引量：1
2马悦,宋联荣,刘国盛,李峻峰,颜贵龙,赖雪飞.二氧化锆:一种多用途的高性能新材料[J].当代化工研究,2021(1):134-138. 被引量：3
3宋健清,李玉虎,张敏,孙亮.直接热解法制备棒状二氧化锆粉体[J].有色金属科学与工程,2022,13(4):28-34.
1吴旭旭,谢光远,吴传栋,时可.分散剂对氧化锆浆料和烧结坯片性能的影响[J].中国粉体技术,2021,27(6):85-91.
2宋健清,李玉虎,张敏,孙亮.直接热解法制备棒状二氧化锆粉体[J].有色金属科学与工程,2022,13(4):28-34.
3周阳,王青春,毛大伟,包金小,宋希文.无铪3YSZ陶瓷材料的显微结构及力学强度[J].辽宁化工,2022,51(9):1190-1193.
4彭艾伊,李俊国,孙旭久.表面处理提高TZP陶瓷韧性研究[J].佛山陶瓷,2022,32(12):17-20.
1朱蕾.辛伐他汀联合盐酸曲美他嗪治疗糖尿病合并冠心病的临床疗效分析[J].中西医结合心血管病电子杂志,2017,5(3):23-23. 被引量：2
2汤力,魏伊,刘凤江,杨波,杨文祥.闭式电液伺服系统泄压时间的一种新用途[J].导弹与航天运载技术,2017(5):71-73.
3卢兆有,王洪国,毛致远,徐秉钺.固体超强酸SO_4^(2-)/ZrO_2的制备及其催化性能研究[J].合成化学,2017,25(11):933-937. 被引量：2
4陈竞生.永利是怎样消化和发展引进技术的?[J].经营与管理,1983,0(4):53-54.
5郭国瑞,范祖恩.利用碱法造纸黑液与废谷糟制造复合肥料的研制报告[J].赣南师范大学学报,1985,0(S1):40-49.
6代德美,刘和义,吴哲,刘聪.直接发泡法制备ZrO_2纤维增强的ZrO_2闭孔泡沫陶瓷[J].真空电子技术,2017,30(5):27-32. 被引量：2
7邓春梅,吴祖件,何兰珍,张国光,吴育廉,温燕梅,康信煌.碱法预处理琼枝麒麟菜提取卡拉胶的工艺优化[J].食品工业科技,2017,38(22):178-183. 被引量：5
8陈雷.浅谈粉煤灰提取氧化铝联产二氧化硅的研究进展[J].化工管理,2017(23):142-144. 被引量：1
9吴刚强,徐绍平,王煜炎,郎中敏,王亚雄.沉淀法制备高比表面超细氧化锆过程结晶动力学[J].无机盐工业,2017,49(11):33-36. 被引量：1
10谢娇娇.溶胶-凝胶法制备ZrO_2/聚苯酯复合材料的性能研究[J].佛山陶瓷,2017,27(11):12-18.
Basic Information:
DOI：
Chinese Library Classification Number:TQ134.12[化学工程—无机化工]
Citation Information:
Zirconium oxychloride was prepared from fused zirconia with the acid-alkali method. The effects were studied of fused zirconia-sodium hydroxide proportion, alkali fusion temperature and alkali fusion time on the conversion rate of zirconium during alkali fusion. The results show that the optimum conditions for alkali fusion are as follows ： mass ratio of fused zirconia to sodium hydroxide 1 ： 1,alkali fusion temperature 790 ℃ and alkali fusion time 1.5 h. Zirconium oxychloride prepared with the above method has a main grade of 36. 25%, Zr recovery rate reaches 91% ,Na2SiO3consumption reduces by more than 98% ,and alkali consumption can be reduced by 52%.
quote
| GB/T 7714-2015 | [1] QI Feng-yuan, BI Hai-yan, SHAO Yue. Experimental Research on Preparation of Zirconium Oxychloride from Fused Zirconia[J]. Rare Metals and Cemented Carbides, 2017(5): 50-52. |
| MLA | [1] QI Feng-yuan, et al., "Experimental Research on Preparation of Zirconium Oxychloride from Fused Zirconia." Rare Metals and Cemented Carbides, no. 5, 2017, pp. 50-52. |
| APA | [1] QI Feng-yuan, BI Hai-yan, & SHAO Yue. (2017). Experimental Research on Preparation of Zirconium Oxychloride from Fused Zirconia. Rare Metals and Cemented Carbides(5), 50-52. |
| IEEE | [1] QI Feng-yuan, BI Hai-yan, and SHAO Yue, "Experimental Research on Preparation of Zirconium Oxychloride from Fused Zirconia," Rare Metals and Cemented Carbides, no. 5, pp. 50-52, 2017. keywords: {zirconium oxychloride;fused zirconia;acid-alkali method;alkali fusion;preparation} |