Determination of Ca,Mg and Mn in Rare Earth Carbonate by ICP-AES AITranslate
Abstract AITranslate
The impurity contents of Ca, Mg and Mn in rare earth carbonate were determined with ICP-AES. The influence of matrix effect was overcome with the standard addition method. The factors affecting determination results were studied, the best analytical spectral lines and the acidity were determined. The detection limit of each element is 0. 003 040. 011 0 μg/mL,the recovery is between 92.85%-101.81%,and the relative standard deviation is between 3.3%- 5.0%. The method is rapid, accurate, convenient and practicable.
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1乔爱香,赵斌,曹磊,江冶.ICP-AES法测定镁合金中微量铜、锰、锌、铝、铁、硅[J].地质学刊,2009,33(3):285-287. 被引量:7
2左良.ICP-AES法测定稀土镁硅铁中铝的测定[J].天津化工,2011,25(6):54-55. 被引量:2
3ThompsonM,WalshJN.ICP光谱分析指南[M].符斌,殷欣平译.北京:冶金工业出版社,1991.
1田春霞,刘文华,刘璟.稀土元素分析[J].分析试验室,2018,37(2):222-248. 被引量:13
1吴伟明,黄智敏,刘乘风.高纯稀土氧化物中其他稀土元素分析[J].中国稀土学报,2018,36(6):641-652. 被引量:5
2杨嘉,段雪梅,程洁红,巢文军.电感耦合等离子体质谱法(ICP-MS)测定土壤和沉积物中37种元素的四种前处理方法探讨[J].江苏理工学院学报,2019,25(2):67-75. 被引量:6
3徐进力,邢夏,唐瑞玲,白金峰,张勤.动能歧视模式电感耦合等离子体质谱法测定地球化学样品中15种稀土元素[J].化学世界,2019,60(9):573-581. 被引量:2
4王宣,李秀兰,周立玉,曾洪亮.高强镁合金的制备研究进展[J].轻合金加工技术,2019,47(11):6-10. 被引量:5
5董学林,何海洋,储溱,仇秀梅,唐兴敏.碱熔沉淀分离-电感耦合等离子体质谱法测定伴生重晶石稀土矿中的稀土元素[J].岩矿测试,2019,38(6):620-630. 被引量:17
6马士精.稀土精矿检测方法[J].化学分析计量,2020,29(1):132-135. 被引量:2
7程林,杨勇,边敏,杨宏伟,刘林,刘海,黄德将,姚敬劬.黄陵断穹核部鳞片石墨矿地球化学特征与成因研究[J].地质与勘探,2020,56(4):745-758. 被引量:7
8王祎亚,高新华,王毅民,邓赛文,李松.地质材料稀土元素的X射线荧光分析文献评介[J].光谱学与光谱分析,2020,40(11):3341-3352. 被引量:1
9胡璇.电感耦合等离子体发射光谱法测定铝土矿中的稀土氧化物[J].岩矿测试,2020,39(6):954-960. 被引量:2
10赵振.三种检测方法测定15种稀土元素总量比对分析[J].福建分析测试,2020,29(6):46-50. 被引量:2
1李先柏,喻庆华.晶型钐、铕、钆、铽碳酸盐的合成[J].稀土,1993,14(5):7-11. 被引量:5
2金斯琴高娃,崔爱端,李玉梅.ICP-AES法测定碳酸稀土、氯化稀土中氧化铕量[J].稀土,2010,31(1):80-82. 被引量:8
3盛华栋.电感耦合等离子体原子发射光谱法测定8种蔬菜中微量元素[J].理化检验:化学分册,2008,44(1):25-27. 被引量:20
4杨仲文,沈灵佳,刘红.美洛昔康中有关物质的HPLC测定[J].中国医药工业杂志,2003,34(11):575-576. 被引量:2
5张蕊,丁兴立,靳灿辉,张建立.气相色谱法测定样品中的残留溶剂[J].河北化工,2004,27(2):60-61. 被引量:1
6魏春艳,丁美英.ICP-AES法测定钢中微量La、Ce、Pr、Nd和Sm[J].稀土,2004,25(5):24-25. 被引量:11
7李帆,丁妍,杨春晟,叶晓英.电感耦合等离子体原子发射光谱法测定纯铼中痕量的铝、镉、铜、镁、锰和钛[J].理化检验:化学分册,2016,52(10):1223-1226. 被引量:9
8李亚琴,陈学清.ICP-OES法测定钽中钙、铝、镁、铌、硅和钨[J].湖南有色金属,2012,28(5):68-69. 被引量:3
9郝丽萍,覃广河,马兰,余琼,贾建平.ICP-AES法测定钆镁合金中钆含量[J].兵器材料科学与工程,2015,38(3):128-130. 被引量:4
10陶俊.ICP-AES法测定铁矿石中钒、钛、铝、铜、锰、砷的研究[J].冶金分析,2005,25(4):64-67. 被引量:16
Basic Information:
DOI:
Chinese Library Classification Number:O657.3[理学—分析化学]
Citation Information:
The impurity contents of Ca, Mg and Mn in rare earth carbonate were determined with ICP-AES. The influence of matrix effect was overcome with the standard addition method. The factors affecting determination results were studied, the best analytical spectral lines and the acidity were determined. The detection limit of each element is 0. 003 040. 011 0 μg/mL,the recovery is between 92.85%-101.81%,and the relative standard deviation is between 3.3%- 5.0%. The method is rapid, accurate, convenient and practicable.
quote
| GB/T 7714-2015 | [1] YI Shi, LIU Rong-li. Determination of Ca,Mg and Mn in Rare Earth Carbonate by ICP-AES[J]. Rare Metals and Cemented Carbides, 2014(5): 68-70. |
| MLA | [1] YI Shi, and LIU Rong-li. "Determination of Ca,Mg and Mn in Rare Earth Carbonate by ICP-AES." Rare Metals and Cemented Carbides, no. 5, 2014, pp. 68-70. |
| APA | [1] YI Shi, & LIU Rong-li. (2014). Determination of Ca,Mg and Mn in Rare Earth Carbonate by ICP-AES. Rare Metals and Cemented Carbides(5), 68-70. |
| IEEE | [1] YI Shi and LIU Rong-li, "Determination of Ca,Mg and Mn in Rare Earth Carbonate by ICP-AES," Rare Metals and Cemented Carbides, no. 5, pp. 68-70, 2014. keywords: {rare earth carbonate;impurity content;ICP-AES;standard addition method} |
