Research on Synthesizing Bi_2S_3 Nanorods by Complex Solvothermal Process AITranslate
Abstract AITranslate
Large-scale Bi2S3 nanorods were synthesized by the complex solvothermal process using copper reagent （sodium diethyldithiocarbamate） as sulfur source,bismuth nitrate as bismuth source,and glycerolwater system as solvent. The product was investigated by X-ray powder diffraction （XRD）,transmission electron microscopy （TEM）,field emission scanning electron microscopy （FESEM） and so on. The results show that the prepared sample is purely of orthorhombic crystal phase. The well-dispersed single-crystal nanorods are obtained, having the lateral sizes of 30-50 nm and the axial sizes of several microns. The formation mechanism of Bi2S3 nanorods is also discussed. It is concluded that both the complex solvent of glycerol-water and the surfactant of PVP have important influences on the morphology and size of Bi2 S3 single -crystal nanorods.
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Basic Information:
DOI：
Chinese Library Classification Number:TB383[一般工业技术—材料科学与工程]
Citation Information:
Large-scale Bi2S3 nanorods were synthesized by the complex solvothermal process using copper reagent （sodium diethyldithiocarbamate） as sulfur source,bismuth nitrate as bismuth source,and glycerolwater system as solvent. The product was investigated by X-ray powder diffraction （XRD）,transmission electron microscopy （TEM）,field emission scanning electron microscopy （FESEM） and so on. The results show that the prepared sample is purely of orthorhombic crystal phase. The well-dispersed single-crystal nanorods are obtained, having the lateral sizes of 30-50 nm and the axial sizes of several microns. The formation mechanism of Bi2S3 nanorods is also discussed. It is concluded that both the complex solvent of glycerol-water and the surfactant of PVP have important influences on the morphology and size of Bi2 S3 single -crystal nanorods.
quote
| GB/T 7714-2015 | [1] YUAN Xin-song, HAO Jian-wen, ZHU Jin-miao, et al. Research on Synthesizing Bi_2S_3 Nanorods by Complex Solvothermal Process[J]. Rare Metals and Cemented Carbides, 2009(3): 5-7. |
| MLA | [1] YUAN Xin-song, et al., "Research on Synthesizing Bi_2S_3 Nanorods by Complex Solvothermal Process." Rare Metals and Cemented Carbides, no. 3, 2009, pp. 5-7. |
| APA | [1] YUAN Xin-song, HAO Jian-wen, ZHU Jin-miao, ZHOU A-yang, & ZHOU Tao. (2009). Research on Synthesizing Bi_2S_3 Nanorods by Complex Solvothermal Process. Rare Metals and Cemented Carbides(3), 5-7. |
| IEEE | [1] YUAN Xin-song, HAO Jian-wen, ZHU Jin-miao, ZHOU A-yang, and ZHOU Tao, "Research on Synthesizing Bi_2S_3 Nanorods by Complex Solvothermal Process," Rare Metals and Cemented Carbides, no. 3, pp. 5-7, 2009. keywords: {complex solvothermal process;Bi2 S3;nanorod;glycerol-water;PVP} |