Simultaneous Determination of Carbon and Sulfur Content in Corrosion Product of Uranium-NioBium Alloy AITranslate
Abstract AITranslate
Combustion-Infrared absorption method is introduced to simultaneously determine carbon and sulfur content in corrosion product of uranium-niobium alloy with LECO CS—444 carbon and sulfur analyzer.The suitable parameters were obtained by carbon and sulfur determination experiments on the synthetic samples of known carbon content.Iron scrap and tungsten particle are selected as a mixed flux.When the sample quantity is 0.150 g,the optimal dosages of iron scrap and tungsten particle are 0.050 g and 1.500 g,respectively.The sulfur detection limit of the said method is 3.6 μg/g.RSD of carbon and sulfur measured values are ≤3.0% and ≤15%,respectively.Standard recovery of carbon and sulfur are 98%~111% and 92%~102%,respectively.
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1姚南红,陈纪光,李建明,胡堪东.HCS-040管式炉红外碳硫分析仪测定稀土金属中碳硫[J].理化检验：化学分册,2002,38(5):251-252. 被引量：6
2陈英.高频红外分析低碳低硫的影响因素[J].理化检验：化学分册,2004,40(5):279-280. 被引量：13
3宵红新;庄艾春.CS-444红外分析仪校正值的研讨[A]北京:力可公司中国办事处,200136-38.
4胡涛;李小杰;齐郁.高频红外吸收测定石灰石中硫的分析方法研究[A]北京:力可公司中国办事处,2001227-229.
5徐本平,易桂华,苗玉艳,牛茂江,钟华.红外碳硫仪测定V_2O_3中的全碳及影响因素[J].钢铁钒钛,1999,20(4):62-66. 被引量：3
6肖红新,陈平.CS-444红外碳硫分析仪空白值的研讨[J].广东有色金属学报,2000,10(1):75-78. 被引量：6
1刘攀,唐伟,张斌彬,李治亚.高频感应燃烧-红外吸收光谱法在分析金属材料中碳、硫的应用[J].理化检验：化学分册,2016,52(1):109-118. 被引量：18
1刘攀,唐伟,张斌彬,李治亚.高频感应燃烧-红外吸收光谱法在测定无机非金属样品中碳、硫的应用[J].理化检验：化学分册,2016,52(4):487-496. 被引量：12
2刘丽娜,刘志民.高频红外法测定碳硫含量在两台碳硫分析仪的应用[J].现代科学仪器,2016,0(5):123-126.
3庄艾春.高频燃烧红外吸收法测定锡锌铅青铜中硫[J].冶金分析,2017,37(4):33-37. 被引量：3
4刘攀,杜米芳,唐伟,张斌彬,李治亚.无机固体样品中硫的测定方法的研究进展[J].理化检验：化学分册,2017,53(8):984-992. 被引量：7
5刘攀,唐伟.高频感应燃烧红外吸收法测定焊接药剂中硫含量[J].冶金分析,2017,37(11):64-68. 被引量：6
6王伟,刘欠,王莹,刘华龙,潘春秀.高温红外吸收光谱法测定煤、焦炭及煤焦油中的硫[J].广州化工,2017,45(22):93-95. 被引量：2
7魏春阳,曾静.高频红外碳硫分析仪对碳化硅质耐火材料中高含量碳化硅的测定[J].中国无机分析化学,2017,7(4):97-101. 被引量：3
8刘攀,杜米芳,唐伟,何鹏飞,董俊轩,张斌彬.无机固体样品中碳的分析方法综述[J].分析仪器,2018(4):8-15. 被引量：3
9齐东子,陈东平,沈文杰.高频燃烧-红外分析仪测定海洋沉积物的总碳含量[J].理化检验：化学分册,2019,55(7):791-795. 被引量：4
10常国梁,刘攀,张毅.高频感应燃烧-红外吸收光谱法测定蒙乃尔镍铜合金中碳[J].冶金分析,2020,40(7):16-21. 被引量：7
1叶信火,汪永静.用测CS—444测定金属中碳和硫若干问题的讨论[J].有色金属分析通讯,1992(2):13-15.
2朗培虹,王建友.HV—21型碳硫分析仪使用注意事项[J].吉林电力技术,1995,8(6):62-63.
3刘博,赵军,杜书涛.LECO CS-200和ELTRA CS-800的性能比较[J].河北冶金,2015(9):68-71.
4邹乐西,吴伦强,向方寿,王林.铀铌合金中微量碳的测定[J].分析试验室,2001,20(3):79-81. 被引量：3
5叶信火,陈蔼舒,汪永静.用CS-444测定金属中碳和硫若干问题的讨论[J].广东有色金属学报,1993,3(2):157-160. 被引量：1
6张晶华.煤气中硫化氢含量的测定[J].山西焦煤科技,2005(7):4-6. 被引量：2
7王为玲.红外吸收法测定镍基高温合金中痕量硫[J].长春工程学院学报：自然科学版,2013,14(4):114-116.
8包钢技术中心红外碳硫仪／氧氮仪／定氢仪[J].包钢科技,2012,38(4).
9刘安春,陈玲华,窦勇,许振良.HCS140型高频红外碳硫分析仪光源的改造[J].冶金设备管理与维修,2006,24(4):43-43.
10苗清.关于磨料及其原材料送检样品取样量的讨论[J].金刚石与磨料磨具工程,1999,19(1):42-43.
Basic Information:
DOI：
Chinese Library Classification Number:TG115.31[金属学及工艺—物理冶金]
Citation Information:
Combustion-Infrared absorption method is introduced to simultaneously determine carbon and sulfur content in corrosion product of uranium-niobium alloy with LECO CS—444 carbon and sulfur analyzer.The suitable parameters were obtained by carbon and sulfur determination experiments on the synthetic samples of known carbon content.Iron scrap and tungsten particle are selected as a mixed flux.When the sample quantity is 0.150 g,the optimal dosages of iron scrap and tungsten particle are 0.050 g and 1.500 g,respectively.The sulfur detection limit of the said method is 3.6 μg/g.RSD of carbon and sulfur measured values are ≤3.0% and ≤15%,respectively.Standard recovery of carbon and sulfur are 98%~111% and 92%~102%,respectively.
quote
| GB/T 7714-2015 | [1] WU Hong-ying, LI Ying-qiu, JI Xin-hua, et al. Simultaneous Determination of Carbon and Sulfur Content in Corrosion Product of Uranium-NioBium Alloy[J]. Rare Metals and Cemented Carbides, 2012(2): 64-67. |
| MLA | [1] WU Hong-ying, et al., "Simultaneous Determination of Carbon and Sulfur Content in Corrosion Product of Uranium-NioBium Alloy." Rare Metals and Cemented Carbides, no. 2, 2012, pp. 64-67. |
| APA | [1] WU Hong-ying, LI Ying-qiu, JI Xin-hua, & WU Mei. (2012). Simultaneous Determination of Carbon and Sulfur Content in Corrosion Product of Uranium-NioBium Alloy. Rare Metals and Cemented Carbides(2), 64-67. |
| IEEE | [1] WU Hong-ying, LI Ying-qiu, JI Xin-hua, and WU Mei, "Simultaneous Determination of Carbon and Sulfur Content in Corrosion Product of Uranium-NioBium Alloy," Rare Metals and Cemented Carbides, no. 2, pp. 64-67, 2012. keywords: {uranium-niobium alloy;corrosion product;carbon and sulfur content;simultaneous determination} |