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Morphology Change of Al_2O_3-doped Molybdenum Alloy Powders AITranslate

School of Materials Science and Engineering, Henan University of Science and Technology;School of Materials Science and Engineering, Henan University of Science and Technology;School of Materials Science and Engineering, Henan University of Science and Technology;School of Materials Science and Engineering, Henan University of Science and Technology
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Publisher: Editorial Office of Rare Metals and Cemented Carbides
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Abstract AITranslate

Alumina-doped molybdenum powders were prepared by hydrothermal synthesis combined with low-temperature calcination and two-stage reduction, and mass fraction of Al2O3 were 0,0. 25%,0. 5%, 0.75% and 1% in the molybdenum alloy powders. The morphology and phase composition of molybdenum alloy powders were analyzed using SEM and XRD,respectively. And the influence of A12 Oa dosage on mo- lybdenum alloy powders was investigated at different preparation stages. The results show that Al2O3 dos- age has a certain effect on the uniformity, particle distribution and particle size of the powders. Increasing Al2O3 content has dispersion effect on aggregation of molybdenum alloy powders. After two-stage hydro- gen reduction, flaky MoOa particles is completely reduced to spherical Mo particles,and the mixed powders are mainly composed of Mo and a-Al2O3 without other phases, α-Al2O3 can refine the molybdenum parti- cles ,and the refinement effect of molybdenum particles is more obvious with alumina increasing.

KeyWords AITranslate

molybdenum alloy powder doping with Al2O3 hydrothermal synthesis morphology

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Basic Information:

DOI:

Chinese Library Classification Number:TG146.412[金属学及工艺—金属材料]

Citation Information:

Alumina-doped molybdenum powders were prepared by hydrothermal synthesis combined with low-temperature calcination and two-stage reduction, and mass fraction of Al2O3 were 0,0. 25%,0. 5%, 0.75% and 1% in the molybdenum alloy powders. The morphology and phase composition of molybdenum alloy powders were analyzed using SEM and XRD,respectively. And the influence of A12 Oa dosage on mo- lybdenum alloy powders was investigated at different preparation stages. The results show that Al2O3 dos- age has a certain effect on the uniformity, particle distribution and particle size of the powders. Increasing Al2O3 content has dispersion effect on aggregation of molybdenum alloy powders. After two-stage hydro- gen reduction, flaky MoOa particles is completely reduced to spherical Mo particles,and the mixed powders are mainly composed of Mo and a-Al2O3 without other phases, α-Al2O3 can refine the molybdenum parti- cles ,and the refinement effect of molybdenum particles is more obvious with alumina increasing.

quote

GB/T 7714-2015 [1] HU Ya-jie, XU Liu-jie, ZHOU Yu-cheng, et al. Morphology Change of Al_2O_3-doped Molybdenum Alloy Powders[J]. Rare Metals and Cemented Carbides, 2014(6): 28-32.
MLA [1] HU Ya-jie, et al., "Morphology Change of Al_2O_3-doped Molybdenum Alloy Powders." Rare Metals and Cemented Carbides, no. 6, 2014, pp. 28-32.
APA [1] HU Ya-jie, XU Liu-jie, ZHOU Yu-cheng, & WEI Shi-zhong. (2014). Morphology Change of Al_2O_3-doped Molybdenum Alloy Powders. Rare Metals and Cemented Carbides(6), 28-32.
IEEE [1] HU Ya-jie, XU Liu-jie, ZHOU Yu-cheng, and WEI Shi-zhong, "Morphology Change of Al_2O_3-doped Molybdenum Alloy Powders," Rare Metals and Cemented Carbides, no. 6, pp. 28-32, 2014. keywords: {molybdenum alloy powder;doping with Al2O3;hydrothermal synthesis;morphology}