Low Temperature and Solid-phase Synthesis and Characterization of Nano-meter Ce-Zr-O Powder AITranslate
Abstract AITranslate
The process for Nano - meter Ce - Zr - O powder preparation was optimized as follows upon investigation of the experimental conditions affecting the product properties through law temperature solid - phase reaction: grinding with ZrOClz(s),Ce2(CO3)3(s),NaOH(s)as raw materials and salicylic acid as complexing agent to obtain precursor, which is dried under room temperature and calcined at 600 ℃ to obtain Nano - meter Ce - Zr - O powder. The sample powder characterization is tested by XRD, TG - DTA, and Raman spectrometer in respect of its particle size, physical phase, thermal stability and Raman feature.
KeyWords AITranslate
1俞建群,贾殿赠,张慧,周蓉,夏熙.CdS纳米粉体的合成新方法——一步室温固相化学反应法[J].化学通报,1998(2):35-37. 被引量:35
2魏坤,何地宝,翟建伟.沉淀法制备稀土氧化物纳米粉体的研究[J].稀土,1999,20(4):27-30. 被引量:28
3贾殿赠,俞建群,夏熙.一步室温固相化学反应法合成CuO纳米粉体[J].科学通报,1998,43(2):172-174. 被引量:62
4Fornasierop Balducci G,et al.Modification of the redox behavior CeO2 induced by structural doping with ZrO2[J].J Catal,1996,164:173.
5Trovarellja Zamar F,et al.Nanophase fluorite-structral CeO2-ZrO2 catalysts prepared by high-energy mechanical milling[J].J Catal,1997,169:490.
1蔡艳华.中低热固相反应研究进展[J].化工技术与开发,2009,38(6):22-28. 被引量:2
1仝其根,白云起,姜怀玺.固相反应生产脱氢醋酸钠物料配比及球磨介质的优化[J].北京工商大学学报:自然科学版,2011,29(3):38-44. 被引量:1
2付江涛,乐治平,黄喜根,王玲玲.固相反应法合成5-取代-8-羟基喹啉偶氮化合物[J].化学试剂,2011,33(10):879-882. 被引量:1
1郝仕油,刘卫东,李良超.流变相-前驱物法制备纳米级Ce-Zr-O粉末的研究[J].功能材料,2004(z1):2789-2791.
2郝仕油,李良超,吕天喜.流变相-前驱物法制备纳米级Ce-Zr-O粉末的研究[J].稀土,2005,26(6):79-82. 被引量:1
3郝仕油,应桃开,周雪珍,李良超.Ce-Zr-O超细粉末制备工艺的优化及其抛光性能[J].稀土,2004,25(1):13-16. 被引量:3
4张志刚,姚广春,马佳,华中胜.低温固相反应合成NiFe_2O_4尖晶石纳米粉[J].东北大学学报:自然科学版,2010,31(6):868-872. 被引量:3
5徐雅南.公司吨钢可比能耗组成及各种影响因素探讨[J].四川冶金,2005,27(6):48-49. 被引量:2
6新建万吨水杨酸进入试产阶段[J].河北冶金,2012(5):69-69.
7储春利,蒋中刚,唐道文.难浸金矿硫脲浸出试验研究[J].有色金属:冶炼部分,2014(3):37-39. 被引量:5
8郝仕油,周雪珍,李良超,应桃开,林秋月.抛光用Ce_(1-x)Zr_xO_2粉末合成工艺的优化及其性能[J].稀有金属,2004,28(4):638-642. 被引量:1
9郝仕油,应桃开,李良超.NH_4HCO_3作沉淀剂制备超细Ce-Zr-O粉末的研究[J].浙江师范大学学报:自然科学版,2005,28(1):42-46. 被引量:1
10林涛,张丽英,赵放,李会谦,吴成义.纳米钨粉坯的低温固相烧结特征[J].机械工程材料,2006,30(5):91-94. 被引量:2
Basic Information:
DOI:
Chinese Library Classification Number:TF123.7[冶金工程—粉末冶金]
Citation Information:
The process for Nano - meter Ce - Zr - O powder preparation was optimized as follows upon investigation of the experimental conditions affecting the product properties through law temperature solid - phase reaction: grinding with ZrOClz(s),Ce2(CO3)3(s),NaOH(s)as raw materials and salicylic acid as complexing agent to obtain precursor, which is dried under room temperature and calcined at 600 ℃ to obtain Nano - meter Ce - Zr - O powder. The sample powder characterization is tested by XRD, TG - DTA, and Raman spectrometer in respect of its particle size, physical phase, thermal stability and Raman feature.
quote
| GB/T 7714-2015 | [1] HAO Shi-you, ZHOU Xue-zhen. Low Temperature and Solid-phase Synthesis and Characterization of Nano-meter Ce-Zr-O Powder[J]. Rare Metals and Cemented Carbides, 2005(3): 9-11. |
| MLA | [1] HAO Shi-you, and ZHOU Xue-zhen. "Low Temperature and Solid-phase Synthesis and Characterization of Nano-meter Ce-Zr-O Powder." Rare Metals and Cemented Carbides, no. 3, 2005, pp. 9-11. |
| APA | [1] HAO Shi-you, & ZHOU Xue-zhen. (2005). Low Temperature and Solid-phase Synthesis and Characterization of Nano-meter Ce-Zr-O Powder. Rare Metals and Cemented Carbides(3), 9-11. |
| IEEE | [1] HAO Shi-you and ZHOU Xue-zhen, "Low Temperature and Solid-phase Synthesis and Characterization of Nano-meter Ce-Zr-O Powder," Rare Metals and Cemented Carbides, no. 3, pp. 9-11, 2005. keywords: {nano - meter;Ce - Zr -O powder;low temperature solid phase;synthsis;characterization} |
