daohang fenxiangbox searchbox qikanlogonew daohangnew searchboxnew navrightzone footerzone paper

Low Temperature and Solid-phase Synthesis and Characterization of Nano-meter Ce-Zr-O Powder AITranslate

Zhejiang Normal University;Nanchang University Rare Earth Engineering Research Center
AITranslate
Publisher: Editorial Office of Rare Metals and Cemented Carbides
Share Citation Information Add to Favorites

    Scan to share on WeChat or Moments

Use WeChat scan.
Share with WeChat friends or Moments

Abstract AITranslate

The process for Nano - meter Ce - Zr - O powder preparation was optimized as follows upon investigation of the experimental conditions affecting the product properties through law temperature solid - phase reaction: grinding with ZrOClz(s),Ce2(CO3)3(s),NaOH(s)as raw materials and salicylic acid as complexing agent to obtain precursor, which is dried under room temperature and calcined at 600 ℃ to obtain Nano - meter Ce - Zr - O powder. The sample powder characterization is tested by XRD, TG - DTA, and Raman spectrometer in respect of its particle size, physical phase, thermal stability and Raman feature.

KeyWords AITranslate

nano - meter Ce - Zr -O powder low temperature solid phase synthsis characterization

1俞建群,贾殿赠,张慧,周蓉,夏熙.CdS纳米粉体的合成新方法——一步室温固相化学反应法[J].化学通报,1998(2):35-37. 被引量:35

2魏坤,何地宝,翟建伟.沉淀法制备稀土氧化物纳米粉体的研究[J].稀土,1999,20(4):27-30. 被引量:28

3贾殿赠,俞建群,夏熙.一步室温固相化学反应法合成CuO纳米粉体[J].科学通报,1998,43(2):172-174. 被引量:62

4Fornasierop Balducci G,et al.Modification of the redox behavior CeO2 induced by structural doping with ZrO2[J].J Catal,1996,164:173.

5Trovarellja Zamar F,et al.Nanophase fluorite-structral CeO2-ZrO2 catalysts prepared by high-energy mechanical milling[J].J Catal,1997,169:490.

1蔡艳华.中低热固相反应研究进展[J].化工技术与开发,2009,38(6):22-28. 被引量:2

1仝其根,白云起,姜怀玺.固相反应生产脱氢醋酸钠物料配比及球磨介质的优化[J].北京工商大学学报:自然科学版,2011,29(3):38-44. 被引量:1

2付江涛,乐治平,黄喜根,王玲玲.固相反应法合成5-取代-8-羟基喹啉偶氮化合物[J].化学试剂,2011,33(10):879-882. 被引量:1

1郝仕油,刘卫东,李良超.流变相-前驱物法制备纳米级Ce-Zr-O粉末的研究[J].功能材料,2004(z1):2789-2791.

2郝仕油,李良超,吕天喜.流变相-前驱物法制备纳米级Ce-Zr-O粉末的研究[J].稀土,2005,26(6):79-82. 被引量:1

3郝仕油,应桃开,周雪珍,李良超.Ce-Zr-O超细粉末制备工艺的优化及其抛光性能[J].稀土,2004,25(1):13-16. 被引量:3

4张志刚,姚广春,马佳,华中胜.低温固相反应合成NiFe_2O_4尖晶石纳米粉[J].东北大学学报:自然科学版,2010,31(6):868-872. 被引量:3

5徐雅南.公司吨钢可比能耗组成及各种影响因素探讨[J].四川冶金,2005,27(6):48-49. 被引量:2

6新建万吨水杨酸进入试产阶段[J].河北冶金,2012(5):69-69.

7储春利,蒋中刚,唐道文.难浸金矿硫脲浸出试验研究[J].有色金属:冶炼部分,2014(3):37-39. 被引量:5

8郝仕油,周雪珍,李良超,应桃开,林秋月.抛光用Ce_(1-x)Zr_xO_2粉末合成工艺的优化及其性能[J].稀有金属,2004,28(4):638-642. 被引量:1

9郝仕油,应桃开,李良超.NH_4HCO_3作沉淀剂制备超细Ce-Zr-O粉末的研究[J].浙江师范大学学报:自然科学版,2005,28(1):42-46. 被引量:1

10林涛,张丽英,赵放,李会谦,吴成义.纳米钨粉坯的低温固相烧结特征[J].机械工程材料,2006,30(5):91-94. 被引量:2

Basic Information:

DOI:

Chinese Library Classification Number:TF123.7[冶金工程—粉末冶金]

Citation Information:

The process for Nano - meter Ce - Zr - O powder preparation was optimized as follows upon investigation of the experimental conditions affecting the product properties through law temperature solid - phase reaction: grinding with ZrOClz(s),Ce2(CO3)3(s),NaOH(s)as raw materials and salicylic acid as complexing agent to obtain precursor, which is dried under room temperature and calcined at 600 ℃ to obtain Nano - meter Ce - Zr - O powder. The sample powder characterization is tested by XRD, TG - DTA, and Raman spectrometer in respect of its particle size, physical phase, thermal stability and Raman feature.

quote

GB/T 7714-2015 [1] HAO Shi-you, ZHOU Xue-zhen. Low Temperature and Solid-phase Synthesis and Characterization of Nano-meter Ce-Zr-O Powder[J]. Rare Metals and Cemented Carbides, 2005(3): 9-11.
MLA [1] HAO Shi-you, and ZHOU Xue-zhen. "Low Temperature and Solid-phase Synthesis and Characterization of Nano-meter Ce-Zr-O Powder." Rare Metals and Cemented Carbides, no. 3, 2005, pp. 9-11.
APA [1] HAO Shi-you, & ZHOU Xue-zhen. (2005). Low Temperature and Solid-phase Synthesis and Characterization of Nano-meter Ce-Zr-O Powder. Rare Metals and Cemented Carbides(3), 9-11.
IEEE [1] HAO Shi-you and ZHOU Xue-zhen, "Low Temperature and Solid-phase Synthesis and Characterization of Nano-meter Ce-Zr-O Powder," Rare Metals and Cemented Carbides, no. 3, pp. 9-11, 2005. keywords: {nano - meter;Ce - Zr -O powder;low temperature solid phase;synthsis;characterization}