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Research on Preparation of Mo-Re Pre-Alloyed Powder by Sol-Gel Method AITranslate

Jiangxi Copper Technology Research Institute Co.,Ltd.;Jiangxi Copper Technology Research Institute Co.,Ltd.;Jiangxi Copper Technology Research Institute Co.,Ltd.;Jiangxi Copper Technology Research Institute Co.,Ltd.
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Publisher: Editorial Office of Rare Metals and Cemented Carbides
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Abstract AITranslate

Mo-47.5Re pre-alloyed powder was prepared by wet chemical sol-gel method with ammonium heptamolybdate tetrahydrate,ammonium perrhenate and anhydrous oxalic acid as raw materials.The ther-mal decomposition and material change rule of wet gel of molybdenum-rhenium precursor during drying-calcination process were studied.Molybdenum-rhenium pre-alloyed powder containing molybdenum matrix phase with solid solution rhenium and molybdenum-rhenium intermediate phase(σ-phase andχ-phase)was prepared.The particles of the pre-alloyed powder are fine,the laser particle size D50 is about 5.09μm,and the distribution of molybdenum and rhenium elements is uniform and highly dispersed.Therefore,it is an ideal powder metallurgy raw material for preparation of molybdenum-rhenium alloy with high rhenium content.

KeyWords AITranslate

sol-gel wet chemical method molybdenum-rhenium alloy pre-alloyed powder thermal decom-position
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Chinese Library Classification Number:TG146.4[金属学及工艺—金属材料]

Citation Information:

Mo-47.5Re pre-alloyed powder was prepared by wet chemical sol-gel method with ammonium heptamolybdate tetrahydrate,ammonium perrhenate and anhydrous oxalic acid as raw materials.The ther-mal decomposition and material change rule of wet gel of molybdenum-rhenium precursor during drying-calcination process were studied.Molybdenum-rhenium pre-alloyed powder containing molybdenum matrix phase with solid solution rhenium and molybdenum-rhenium intermediate phase(σ-phase andχ-phase)was prepared.The particles of the pre-alloyed powder are fine,the laser particle size D50 is about 5.09μm,and the distribution of molybdenum and rhenium elements is uniform and highly dispersed.Therefore,it is an ideal powder metallurgy raw material for preparation of molybdenum-rhenium alloy with high rhenium content.

quote

GB/T 7714-2015 [1] CHEN Ri-kui, LI Song-bin, FENG Yong-shan, et al. Research on Preparation of Mo-Re Pre-Alloyed Powder by Sol-Gel Method[J]. Rare Metals and Cemented Carbides, 2024(5): 13-17.
MLA [1] CHEN Ri-kui, et al., "Research on Preparation of Mo-Re Pre-Alloyed Powder by Sol-Gel Method." Rare Metals and Cemented Carbides, no. 5, 2024, pp. 13-17.
APA [1] CHEN Ri-kui, LI Song-bin, FENG Yong-shan, & LI Ge-ping. (2024). Research on Preparation of Mo-Re Pre-Alloyed Powder by Sol-Gel Method. Rare Metals and Cemented Carbides(5), 13-17.
IEEE [1] CHEN Ri-kui, LI Song-bin, FENG Yong-shan, and LI Ge-ping, "Research on Preparation of Mo-Re Pre-Alloyed Powder by Sol-Gel Method," Rare Metals and Cemented Carbides, no. 5, pp. 13-17, 2024. keywords: {sol-gel;wet chemical method;molybdenum-rhenium alloy;pre-alloyed powder;thermal decom-position}