Study on Tantalum and Niobium Recovery by Acid Leaching and Sodium Alkali Fusing from Tungsten Residue AITranslate
Abstract AITranslate
The enrichment and recovery of tantalum and niobium through acid leaching and sodium alkali fusing from tungsten residue is studied. When 5 % HCl consumption amounts to 2.5 times of the theoretical value,reaction temperature is 40 ℃ and reaction time is 30 min,72.1% of the iron and 74.7% of the manganese can be removed and the recovery of tantalum and niobium are 92% and 84.6% respectively. Then the acid leach residue was fused in NaOH and Na2CO3. When the mass ratio of acid leach residue to alkali is 3 : 2 and reaction time is 60 min,the content of Ta2O5 and Nb2O5 in the product could be 0.48% and 2.74% respectively. And the recovery of tantalum and niobium are 83 % and 74.8 % respectively. The total recoveries of tantalum and niobium are 76.4% and 63.3% respectively. It shows that tantalum and niobium can be effectively enriched and recovered from tungsten residue by acid leach and sodium alkali fusing.
KeyWords AITranslate
1夏文堂.钨的二次资源及其开发前景[J].再生资源研究,2006(1):11-17. 被引量:25
2罗教生,王莉莉,王冠亚.钨渣的综合利用研究[J].江西冶金,1998,18(6):31-32. 被引量:6
3吴铭.钽铌冶金工艺学[M].北京:中国有色金属工业总公司职工教育教材编审办公室,1986.36-53.
4戴艳阳,钟海云,李荐,钟晖.钨渣中有价金属综合回收工艺[J].中南工业大学学报,2003,34(1):36-39. 被引量:24
5何万年.浅谈低品位钽铌矿的富集.稀有金属,1980,(2):64-72.
6秦光荣.铌钽溶液的性质及其反应特性.分析化学,1978,(6):115-130.
1朱海玲,邓海波,吴承桧,何小民.钨渣的综合回收利用技术研究现状[J].中国钨业,2010,25(4):15-18. 被引量:25
2向仕彪,黄波,王晓辉,郑诗礼.从废钨渣中酸法回收钽铌的研究[J].有色冶金设计与研究,2012,33(2):5-7. 被引量:15
3肖超,刘景槐,吴海国.低品位钨渣处理工艺试验研究[J].湖南有色金属,2012,28(4):24-26. 被引量:19
4杨秀丽,王晓辉,向仕彪,孙青,魏昶,郑诗礼.盐酸法富集钨渣中的钽和铌[J].中国有色金属学报,2013,23(3):873-881. 被引量:21
5汪加军,王晓辉,黄波,郑诗礼.废钨渣中钽、铌、钨高效共提新工艺研究[J].有色金属科学与工程,2013,4(5):91-96. 被引量:12
6杨新华,许亮,周洁英,欧阳红,陈冬英.钨钽铌粗精矿碱分解试验研究[J].中国钨业,2013,28(6):38-41. 被引量:5
7谢晓霞,张幸幸.我国钨渣回收利用研究现状和发展趋势[J].上海化工,2014,39(5):26-29. 被引量:7
8苏正夫,刘宇晖.钨渣中钨回收利用新工艺研究[J].稀有金属与硬质合金,2014,42(4):11-13. 被引量:13
9汪加军,王晓辉,张盈,郑诗礼.含钽铌废渣中钽铌资源的综合回收工艺研究[J].稀有金属,2015,39(3):251-261. 被引量:11
10杨少华,王君,谢宝如,赖晓晖,王浩然.低品位钨渣处理工艺[J].有色金属科学与工程,2015,6(6):29-32. 被引量:10
1史明,唐忠阳,陈星宇.现代钨冶炼过程中废水处理现状与发展[J].稀有金属与硬质合金,2015,43(2):1-5. 被引量:6
2曾坚贤,孙霞辉,周虎,贺勤程,李书.聚电解质强化超滤技术处理钨(Ⅵ)[J].过程工程学报,2011,11(3):396-400. 被引量:5
3肖超,刘景槐,吴海国.低品位钨渣处理工艺试验研究[J].湖南有色金属,2012,28(4):24-26. 被引量:19
4杨秀丽,王晓辉,向仕彪,孙青,魏昶,郑诗礼.盐酸法富集钨渣中的钽和铌[J].中国有色金属学报,2013,23(3):873-881. 被引量:21
5孟晗琪,马光,陈昆昆,王靖坤.钨钽的氧化碱浸分离实验研究[J].广州化工,2013,41(16):1-2.
6汪加军,王晓辉,黄波,郑诗礼.废钨渣中钽、铌、钨高效共提新工艺研究[J].有色金属科学与工程,2013,4(5):91-96. 被引量:12
7谢刚,田林.2013年云南冶金年评[J].云南冶金,2014,43(2):42-53.
8杜阳,马光,吴贤,操齐高.碱熔融—水浸法分离钨的试验研究[J].有色金属:冶炼部分,2014(5):34-37. 被引量:6
9刘云峰,唐娴敏,陈滨.金属钪资源及我国回收利用技术[J].湖南工业大学学报,2014,28(2):56-61. 被引量:9
10杨秀丽,张军伟,方夕辉.低品位铌矿硫酸焙烧——草酸浸出回收铌[J].有色金属工程,2014,4(3):48-50. 被引量:4
1肖刘萍,孙应.镍钼矿钼交后液中提取镍的研究[J].矿冶,2009,18(4):44-46. 被引量:1
2戴艳阳,钟晖,钟海云.钨渣中钽铌回收研究[J].有色金属,2009,61(3):87-89. 被引量:16
3张寒,李凌云,李玉,吕燕鸣.钛、铬、钒的联合测定[J].莱钢科技,2016,0(1):65-68.
4刘斌莲,魏洪洁,王宝文.铅电解阳极泥中锑铋的浸出试验[J].矿产综合利用,2013(2):48-50. 被引量:2
5马光强,邹敏.用盐酸浸出含钛高炉渣富集钛的试验研究[J].湿法冶金,2015,34(1):46-49. 被引量:3
6孔祥峰,杨斌,熊恒,燕春培,聂博,闫华龙,徐宝强,刘大春.粗铅真空蒸馏脱除铜锡的研究[J].真空科学与技术学报,2014,34(5):522-527. 被引量:3
7张俊,严定鎏,齐渊洪.钒钛磁铁矿利用新工艺的理论分析[J].钢铁钒钛,2015,36(3):1-5. 被引量:5
8吴卫煌.氯酸钠分金试验研究及工业应用[J].黄金,2017,38(3):68-70. 被引量:2
9谭代娣,蒋朝金,杨跃新,邓涛.从铋渣中回收铜铋实验研究[J].矿冶工程,2016,0(6):100-103. 被引量:8
10刘猛,吴金玲,杨飞,黄文孝.含钒铝土矿中钒高效浸出实验研究[J].山东化工,2015,44(18):112-115. 被引量:1
Basic Information:
DOI:
Chinese Library Classification Number:TF841.6[冶金工程—有色金属冶金]
Citation Information:
The enrichment and recovery of tantalum and niobium through acid leaching and sodium alkali fusing from tungsten residue is studied. When 5 % HCl consumption amounts to 2.5 times of the theoretical value,reaction temperature is 40 ℃ and reaction time is 30 min,72.1% of the iron and 74.7% of the manganese can be removed and the recovery of tantalum and niobium are 92% and 84.6% respectively. Then the acid leach residue was fused in NaOH and Na2CO3. When the mass ratio of acid leach residue to alkali is 3 : 2 and reaction time is 60 min,the content of Ta2O5 and Nb2O5 in the product could be 0.48% and 2.74% respectively. And the recovery of tantalum and niobium are 83 % and 74.8 % respectively. The total recoveries of tantalum and niobium are 76.4% and 63.3% respectively. It shows that tantalum and niobium can be effectively enriched and recovered from tungsten residue by acid leach and sodium alkali fusing.
quote
| GB/T 7714-2015 | [1] ZHANG Li, ZHONG Hui, DAI Yan-yang. Study on Tantalum and Niobium Recovery by Acid Leaching and Sodium Alkali Fusing from Tungsten Residue[J]. Rare Metals and Cemented Carbides, 2008(2): 6-9. |
| MLA | [1] ZHANG Li, et al., "Study on Tantalum and Niobium Recovery by Acid Leaching and Sodium Alkali Fusing from Tungsten Residue." Rare Metals and Cemented Carbides, no. 2, 2008, pp. 6-9. |
| APA | [1] ZHANG Li, ZHONG Hui, & DAI Yan-yang. (2008). Study on Tantalum and Niobium Recovery by Acid Leaching and Sodium Alkali Fusing from Tungsten Residue. Rare Metals and Cemented Carbides(2), 6-9. |
| IEEE | [1] ZHANG Li, ZHONG Hui, and DAI Yan-yang, "Study on Tantalum and Niobium Recovery by Acid Leaching and Sodium Alkali Fusing from Tungsten Residue," Rare Metals and Cemented Carbides, no. 2, pp. 6-9, 2008. keywords: {tungsten residue;acid leach;sodium alkali fusing;tantalum and niobium;recovery} |
