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Study on Microstructure of Zr-1Nb-0.1Fe-0.1Cu Zirconium Alloy AITranslate

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Publisher: Editorial Office of Rare Metals and Cemented Carbides
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Abstract AITranslate

Zr-1 Nb-0.1 Fe-0.1 Cu plate samples with a thickness of 1.4 mm were prepared with sponge zirconium by electrode pressing,vacuum consumable arc melting,forging,homogenization treatment,quenching,hot rolling,multi-pass cold rolling and annealing.The metallographic microstructure of Zr-1 Nb-0.1 Fe-0.1 Cu alloy and the composition,size,structure and distribution of the second phase were analyzed by OM,SEM and TEM.The test results show that the metallographic microstructure of Zr-1 Nb-0.1 Fe-0.1 Cu alloy annealed at 580℃for 2 h is basically recrystallized equiaxed crystal,the grain size grade is 13,and the average grain size is less than 6μm.Elliptical second-phase particles are precipitated and dispersed in the grains and grain boundary of the alloy.More than 95%of the second-phase particles have smaller size than 200 nm.There are three kinds of second-phase particles in Zr-1 Nb-0.1 Fe-0.1 Cu alloy,includingβ-Nb precipitate with a large content,a grain size of less than 100 nm,and bcc structure,(Zr,Nb)2Fe precipitate with a less content,a grain size of less than 200 nm,and hcp structure,and Zr;Cu precipitate with the least content,a greater grain size than 200 nm,and tetragonal structure.

KeyWords AITranslate

zirconium alloy microstructure the second phase grain size Zr-Nb-Fe-Cu

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Basic Information:

DOI:

Chinese Library Classification Number:TG146.4[金属学及工艺—金属材料]

Citation Information:

Zr-1 Nb-0.1 Fe-0.1 Cu plate samples with a thickness of 1.4 mm were prepared with sponge zirconium by electrode pressing,vacuum consumable arc melting,forging,homogenization treatment,quenching,hot rolling,multi-pass cold rolling and annealing.The metallographic microstructure of Zr-1 Nb-0.1 Fe-0.1 Cu alloy and the composition,size,structure and distribution of the second phase were analyzed by OM,SEM and TEM.The test results show that the metallographic microstructure of Zr-1 Nb-0.1 Fe-0.1 Cu alloy annealed at 580℃for 2 h is basically recrystallized equiaxed crystal,the grain size grade is 13,and the average grain size is less than 6μm.Elliptical second-phase particles are precipitated and dispersed in the grains and grain boundary of the alloy.More than 95%of the second-phase particles have smaller size than 200 nm.There are three kinds of second-phase particles in Zr-1 Nb-0.1 Fe-0.1 Cu alloy,includingβ-Nb precipitate with a large content,a grain size of less than 100 nm,and bcc structure,(Zr,Nb)2Fe precipitate with a less content,a grain size of less than 200 nm,and hcp structure,and Zr;Cu precipitate with the least content,a greater grain size than 200 nm,and tetragonal structure.

quote

GB/T 7714-2015 [1] QU Jing-wen, LEI Jiang, SHI Ming-hua, et al. Study on Microstructure of Zr-1Nb-0.1Fe-0.1Cu Zirconium Alloy[J]. Rare Metals and Cemented Carbides, 2022(2): 57-63.
MLA [1] QU Jing-wen, et al., "Study on Microstructure of Zr-1Nb-0.1Fe-0.1Cu Zirconium Alloy." Rare Metals and Cemented Carbides, no. 2, 2022, pp. 57-63.
APA [1] QU Jing-wen, LEI Jiang, SHI Ming-hua, ZHOU Jun, LI Yu-li, & ZHANG Hai-xia. (2022). Study on Microstructure of Zr-1Nb-0.1Fe-0.1Cu Zirconium Alloy. Rare Metals and Cemented Carbides(2), 57-63.
IEEE [1] QU Jing-wen, LEI Jiang, SHI Ming-hua, ZHOU Jun, LI Yu-li, and ZHANG Hai-xia, "Study on Microstructure of Zr-1Nb-0.1Fe-0.1Cu Zirconium Alloy," Rare Metals and Cemented Carbides, no. 2, pp. 57-63, 2022. keywords: {zirconium alloy;microstructure;the second phase;grain size;Zr-Nb-Fe-Cu}