Microwave Digestion and Zirconium Determination of Al-Zr Alloy AITranslate
Abstract AITranslate
Al-Zr alloy with high zirconium content was digested through the household microwave oven and HCl-H2O2 system,and Zr content was titrated with EDTA.The conditions of microwave digestion were optimized through single factor experiments and orthogonal experiments.Compared with traditional methods,microwave digestion is characterized by fast digestion,simple operation,less sample loss and more accurate determination of Zr content.The Zr recovery is 97.11%～102.81%,and the relative standard deviation（n=5） 0.11%～0.13%.
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Basic Information:
DOI：
Chinese Library Classification Number:TG146.414[金属学及工艺—金属材料]
Citation Information:
Al-Zr alloy with high zirconium content was digested through the household microwave oven and HCl-H2O2 system,and Zr content was titrated with EDTA.The conditions of microwave digestion were optimized through single factor experiments and orthogonal experiments.Compared with traditional methods,microwave digestion is characterized by fast digestion,simple operation,less sample loss and more accurate determination of Zr content.The Zr recovery is 97.11%～102.81%,and the relative standard deviation（n=5） 0.11%～0.13%.
quote
| GB/T 7714-2015 | [1] ZHOU Xi-lin, YIN Ji-xian, LIU Ji-yong, et al. Microwave Digestion and Zirconium Determination of Al-Zr Alloy[J]. Rare Metals and Cemented Carbides, 2010(4): 56-59. |
| MLA | [1] ZHOU Xi-lin, et al., "Microwave Digestion and Zirconium Determination of Al-Zr Alloy." Rare Metals and Cemented Carbides, no. 4, 2010, pp. 56-59. |
| APA | [1] ZHOU Xi-lin, YIN Ji-xian, LIU Ji-yong, & CHEN Wen. (2010). Microwave Digestion and Zirconium Determination of Al-Zr Alloy. Rare Metals and Cemented Carbides(4), 56-59. |
| IEEE | [1] ZHOU Xi-lin, YIN Ji-xian, LIU Ji-yong, and CHEN Wen, "Microwave Digestion and Zirconium Determination of Al-Zr Alloy," Rare Metals and Cemented Carbides, no. 4, pp. 56-59, 2010. keywords: {Al-Zr alloy;microwave digestion;Zirconium determination;EDTA titration} |